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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> AJMcCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
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<br /> ht //www mecam bell com E-mail main@mccampbell com
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<br /> GEOSOLV, LLC Client Project ID Nunatl/Jernigan Date Sampled 02/20-03/01/01
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Client P O Date Analyzed 03/05-03/08/01
<br />' EPA method 8250 Volatile Organics By GC/MS
<br /> Lab ID 61492
<br /> Client ID MW-1 30" -31
<br /> Matrix S
<br /> Compound Concentration* Rcportmg Limit * itcportrng Limn
<br /> W S
<br /> p Compound Concentration
<br /> W I S
<br /> Acetone tbi ND<35 70 25 trans-],3-Dichloropmpene ND 10 50
<br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 50
<br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND 10 50
<br /> Bromochloromethane ND 10 50 Hexachlorobutadiene ND 50 25
<br /> Bromodichloromethane ND 10 50 lodomethane ND 10 50
<br /> Bromoform ND 10 50 Isopropylbenzene ND 10 50
<br /> Bromomethane ND 10 50 p-lsopropyl toluene ND 10 50
<br /> n-Butyl benzene ND ] 0 50 Methyl butyl ketone ND 10 50
<br /> sec-Butyl benzene ND 1 0 50 Methylene Chloride` ND 10 50
<br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10
<br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketone a ND ]0 50
<br /> Metha
<br /> Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) --- 10 50
<br /> enzene ND 1 0 5 0 Naphthalene ND 50 50
<br /> thane ND 10 5 0 n-Propyl benzene ND 10 50
<br /> oethyl Vinyl Ether` ND 1 0 5 0 Styrene ND 1 0 so
<br /> orm ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 10 50
<br /> ethane ND l 0 5 0 1,1,2,2-Tetrachloroethane ND 10 50
<br /> toluene ND 1 0 5 0 Tetrachloroethene ND 1 0 50
<br /> toluene ND ] 0 5 0 Toluene 77 10 50
<br /> chloromethane ND 1 0 5 0 1,2,3-Trichlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 50 25
<br /> Dibromomethane ND 1 0 5 0 1,1,1-Tnchloroethane ND 10 50
<br /> 12-Dichlorobenzene ND 10 50 1,1,2-Trichloroethane ND 10 50
<br />' 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND 10 50
<br /> I,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 10 50
<br /> Dichlorodifluoromethane ND _]_o —3-0— 1,2,3-Trichloropropane ND 10 50
<br /> 1 1-Dichloroethane ND 1 0 50 1,2,4-Trimethylbenzene ND 10 50
<br /> 1,2-Dichloroethane ND __f_0_ 50 i,3,5-Trimethylbenzene ND 10 50
<br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate ° ND 50 25
<br /> cis-1,2-Dichloroethene ND 10 50 Vinyl Chloride " ND 10 50
<br /> trans-1,2-Dichloroethene ND 10 50 Xylenes,total ND 10 so
<br /> 1,2 Dichloropropane ND 1 Q 1 50 Comments
<br /> 1,3-Dichloropropane ND 1 05 0 Surrogate Recoveries
<br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 102
<br /> 1,1-Dichloropropene ND 1 0 5 0 Toluene-d8 109
<br /> cis-1,3-Dichloropropeiie ND 1 0 5 0 4-BromoOuorobenzene 96
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2 hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol %
<br /> sediment, (]) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton, Lab Director
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