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I 10 2nd Avenue South,#ED7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> IF44 ht //WWW mccam bell com E-mail main@mccampbell com
<br /> GEDSOLV,LLC Client Project ID Nunan/Jernigan Date Sampled 02120-03/01101
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Client P O Date Analyzed 03105-03/08101
<br /> EPA method 8260 Volatile Organics By GC/MS
<br /> Lab ID 61495
<br /> Client ID MW-1 60"2-61
<br /> Matrix S
<br /> Compound Concentration* Reporting Limn * Reporting Limit
<br /> W S
<br /> P Compound Concentration*
<br /> W I S
<br /> Acetone(b) ND<35 50 25 trans-l,3-Dichloropropene ND 10 50
<br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 50
<br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 10 5 0
<br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25
<br /> Bromodichloromethane ND 10 5 0 lodomethane ND 10 5 0
<br /> Bromoform ND 1 0 5 0 lsopropylbenzene ND 1 0 5 0
<br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 5 0
<br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 10 50
<br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chloride"' ND 10 5 0
<br /> tert-Butyl benzene ND 1 0r5O
<br /> Methyl ethyl ketone ND 20 10
<br /> Carbon Disulfide ND 1 0 Methyl isobutyl ketone g ND 10 50
<br /> Carbon Tetrachloride ND 1 0 Methyl tert-Butyl Ether(MTBE) --- to 5 0
<br /> Chlorobenzene ND 10 Naphthalene ND 50 50—
<br /> Chloroethane
<br /> DChloroethane ND 1 0 n-Propyl benzene ND 1 0 5 0
<br /> 2-Chloroethyl Vinyl Ether(c) ND 1 p Styrene ND 10 50
<br /> Chloroform ND 1 0 1 50 1,1,1,2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 10 50
<br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND 10 5 0
<br /> 4-Chlorotoluene ND 1 0 5 0 7 oluene 22 1 0 5 0
<br /> Dibromochloromethane ND 1 0 50 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Trichlorobenzene ND 5 0 25
<br /> Dibromomethane ND 1 0 5 0 1,1,1-Trichloroethane ND 10 5 0
<br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Trichloroethane ND 10 50
<br /> 1,3-Dichlorobenzene ND 1 0 5 0 Tnchloroethene ND 10 50
<br /> 3,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 10 5 0
<br /> Dichlorodifluoromethane ND to 50 1,2,3-Tnchloropropane PND
<br /> 10 5 0
<br /> 1,1-Dichloroethane ND l0 50 1,2,4-Tnmethylbenzene 10 50
<br /> I 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Trimethylbenzene 1 0 5 0
<br /> 1,1-Dichloroethene ND 1 0 50 Vinyl Acetate 5 0 25
<br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride " 10 5 0
<br /> trans-1,2-Dichloroethene ND 1 V05
<br /> Xylenes,total 10 50
<br /> 1 2-Dichloropropane ND 1 Comments
<br /> 1,3-Dichloropropane ND ! Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND l Dibromofluoromethane 101
<br /> l,l-Dwhloropropene ND 1Toluene-d8 108
<br /> cis-],3Dtchlaropropene ND 14-Bromofluorobenzene 97
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> • pentanone or isopropylacetone (h)lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene (o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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