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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> ht //wca
<br /> ww mcm bell com E-mail main@mccampbell coin
<br /> GEOSOLV,LLC Client Project ID Nunan/jernigan Date Sampled 02/20-03/01/01
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Client P O Date Analyzed 03105-03/08/01
<br /> Volatile Organics By GUMS
<br /> EPA method 8260
<br /> Lab ID 61510
<br /> Client ID MW-2 38-38
<br /> Matrix S
<br /> Reporting Limit Reporting Limit
<br /> Compound Concentration* W S Compound Concentration* W 5
<br /> Acetone(e) ND<35 50 25 trans-1,3-Dichloropropene ND l 0 50
<br /> Benzene ND 1 0 50 Ethylene dibromide ND 1 0 50
<br /> Bromobeiizene ND 10 50 Ethylbenzene ND 10 50
<br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25
<br /> Bromodichloromethane ND 10 50 lodomethane ND 10 50
<br /> Bromoform ND 10 50 ]sopropylbenzene ND 1 0 5 0
<br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 1 0 50
<br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND to 5 0
<br /> sec-Butyl benzene ND 10 50 Methylene Chlonde` ND 10 50
<br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketones ND 1 0 50
<br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) --- 10 50
<br /> Chlorobenzene ND 10 5 0 Naphthalene ND 5 0 50
<br /> Chloroethane ND 10 5 0 n-Propyl benzene ND 10 50
<br /> 2-Chloroethyl Vinyl Ether"' ND 10 5 0 Styrene MND 10 50
<br /> Chloroform ND 10 5 0 1,1,1,2-Tetrachloroethane ND 1 0 50
<br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 10 50
<br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 10 50
<br /> 4-Chlorotoluene ND 1 0 5 0 Toluene 9T 27 10 50
<br /> Dibromochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 5 0 25
<br /> Dibromomethane ND 10 5 0 1,1,1-Tnchloroelhane ND 10 5 0
<br /> 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Trichloroethane ND 10 5 0
<br /> 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 10 50
<br /> 1,4-Dichlorobenzene ND l 0 5 0 Trichlorofluoromethane ND 10 50
<br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tnchloropmpane ND 10 50
<br /> l,l-Dichloroethane ND I0 50 12,4-Tnrnethylbenzene 11 10 50
<br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Tnmethylbenzene„ j ND 10 50
<br /> 1,1-Dichloroethene ND 1 0 5 0 Vinyl Acetate m ND 5 0 25
<br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride ” ND 10 5 0
<br /> trans-1,2-Dichloroethene ND 1 0 5 0 Xylenes,total 9 2 10 so
<br /> 1,2-Dichloropropane ND 10 50 Comments
<br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries{%)
<br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 97
<br /> 71-Dtchlompropene ND 1 0 50 Toluene-d8 105
<br /> cis-1,3-Dichloropropene ND 10 50 4-Bromofluorobenzene 118
<br /> water and vapor samples are reported in ugly,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hcxanone (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol %
<br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester (n)
<br /> chlomethene,(o)dimethylbenzenes
<br />' DHS Certification No 1644 Edward Hamilton,Lab Director
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