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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//www mccampbell co m E-mail mam@mccampbell cam
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<br /> GEOSOLV,LLC Client Project ID Nunan/Jernigan Date Sampled 02/20-03/01/01
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Client P 0 Date Analyzed 03105-03108101
<br /> Volatile Organics By GUMS
<br /> EPA method 8260
<br /> Lab ID 61511
<br /> Client ID MW-2 45"46
<br /> Matrix S
<br /> Reporting Limn Reporting Limit
<br /> Compound Concentration* W 5 Compound Concentration* W S
<br /> Acetone cui ND<35 50 25 trans-l,3-Dichloropropene ND 10 50
<br /> Benzene ND 1 0 5 0 Ethylene dibromide ND 1 0 5 0
<br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND 1 0 5 0
<br /> Bromochloromethane ND 1 0 5 0 Hexachlorobutadiene ND 5 0 25
<br /> Bromodichloromethane ND 1 0 5 0 lodomethane ND 1 0 5 0
<br /> Bromoform ND 1 0 5 0 Isopropylbenzene ND 1 0 5 0
<br /> Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 1 0 5 0
<br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 1 0 5 0
<br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chloride"' ND 1 0 5 0
<br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone 17 2 0 10
<br /> Carbon Disulfide ND 1 0 5 0 Methyl isobutyl ketone a ND 1 0 5 0
<br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) --- 1 0 5 0
<br /> Chlorobenzene ND 1 0 5 0 Naphthalene ND 5 0 5 0
<br /> Chloroethane ND 1 0 5 0 n-Propyl benzene ND 1 0 5 0
<br /> 2-Chloroethyl Vinyl Ethe ND 1 0 5 0 Styrene W ND 1 0 5 0
<br /> Chloroform ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 1 0 5 0
<br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 1 0 5 0
<br /> 2 hilorotoluene ND 1 0 5 0 Tetrachloroethene ND 1 0 5 0
<br /> 4-Chlorotoluene ND 1 0 5 0 Toluene 110 1 0 5 0
<br /> Dibromochloromethane ND 1 0 5 0 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25
<br /> Dibromomethane ND 1 0 5 0 1,1,1-Trichloroethane ND 1 0 5 0
<br /> 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2-Trichloroethane ND 1 0 5 0
<br /> 1,3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 1 0 5 0
<br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 1 0 5 0
<br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Trichloropropane ND 10 5 0
<br /> 1,1-Dichloroethane ND 1 0 5 0 1,2,4-Trimethykbenzene ND 1 0 5 0
<br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Tnmethylbenzene ND 1 0 5 0
<br /> IJ-Dichloroethene ND 1 0 5 0 Vinyl Acetate " ND 5 0 25
<br /> cis-1 2-Dichloroethene ND 1 0 5 0 Vinyl Chloride ND 1 0 5 0
<br /> trans-1,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 1 0 5 0
<br /> 1,2-Dichloropropane ND 1 0 5 0 Comments
<br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 98
<br /> 1,1-Dichloropropene ND 1 0 50 Toluene-d8 105
<br /> cis-1,3-Dichloropropene ND 1 0 5 0 4-Bromofluorobenzene 121
<br /> water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloreethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (1) 2-butanone (g) 4-methyl-2-
<br /> pentanone or isopropy]acetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than --5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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