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1 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell corn E-mail main@mccampbell corn <br /> 1 GEOSOLV,LLC Client Project 1D Nunaii/Jernigan Date Sampled 02120-03/01101 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Client P O Date Analyzed 03/05-03/08/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 61516 <br /> Client ID MW-2 83"'-84 <br /> Matrix S <br /> Compound Concentration* Repaning Limit Compound Concentration* ReW mng Limit <br /> 1 W S W S <br /> Acetone mt ND<35 50 25 trans-l,3-Dichloropropene ND 10 50 <br /> Benzene ND 10 5 0 Ethylene dibromide ND 10 5 0 <br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 10 5 0 <br /> Bromochloromethane ND 10 50 Hexachlorobutadiene ND 5 0 25 <br /> BTomodlchloromethane ND 10 5 0 lodomethane ND 10 5 0 <br /> Bromoform ND 1 0 5 0 Isopropylbenzene ND 10 5 0 <br /> Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 10 5 0 <br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 10 5 0 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chloridet') ND 10 5 0 <br /> ter(-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone'8) ND 10 50 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) --- 10 50 <br /> Chlorobenzene ND 1 0 5 0 Naphthalene ND 50 5 0 <br /> Chloroethane ND 1 0 5 0 n-Propyl benzene ND 10 5 0 <br /> 2-Chloroethyl Vinyl Ether"' ND 1 0 5 0 Styrene ND 1 0 5 0 <br /> Chloroform ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 1 0 5 0 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 10 5 0 <br /> 4-Chlorotoluene ND 1 0 5 0 Toluene W 20 10 5 0 <br /> Dibromoehloromethane ND 1 0 50 1,2,3-Trichlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 50 1,1,1-Tnchloroethane ND 10 50 <br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Trichloroethane ND 10 50 <br /> 1 3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Trichloropropane ND 10 5 0 <br /> 1,1-Dicbloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Trtmethylbenzene ND 10 50 <br /> I,1-Dichloroethene ND 10 5 0 Vinyl Acetate ro ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chloride in) ND 10 5 0 <br /> trans-l,2-Dichloroethene ND 10 5 0 Xylenes,total ND 10 50 <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%} <br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 98 <br /> 1,1-Dtchloropropene ND 10 50 Toluene-d8 106 <br /> c1s-1,3 Dtchloropropene ND A-10 1 50 4-Bromofluorobenzene 115 <br /> water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit NIA means analyte not applicable(o this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (1)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />