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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//w%vwmccampbell com E-mail main@mccampbell com <br /> GEOSOLV, LLC Client Project ID Nunan/Jernigan Date Sampled 02120-03/01/01 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Client P O Date Analyzed 03105-03/08/01 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab 1D 61514 <br /> Client ID MW-2 60" -61 <br /> M atnx S <br /> Reputing Limit Reporting Limit <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone M NIX35 50 25 trans-l,3-Dichloropropene ND 10 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 50 <br /> Bromobenzene ND 1 0 5 6 Etbylbenzene ND 10 50 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 10 50 <br /> Bromoform ND 1 0 50 Isopropylbenzene ND 10 50 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chloride"' ND 10 50 <br /> tent-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 1 0 50 Metbyl isobutyl ketones ND 10 50 <br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butyl Ether(MTBE) --- 10 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 50 <br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 10 50 <br /> 2 Chloroethyl Vinyl Me ND 1 0 50 Styrene ND 1 0 50 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 1 0 5 0 <br /> 4-Chlorotoluene NO 10 50 Toluene 32 10 5 0 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlombenzene ND 50 25 <br /> 1,2-D3bromo-3-chloropropane ND 20 10 1,2,4-Tncblorobenzene ND 50 25 <br /> Dibromomethane ND 10 5 0 1,1,i-Trichloroethane ND 10 5 0 <br /> 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Tnchloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 10 50 <br /> 1,4-D3chlorobenzene ND 10 5 0 Tnehlorofluoromethane ND 10 5 0 <br /> Dtchlorodifluoromethane ND 10 50 1,2,3-Tnchloropropane ND 10 50 <br /> I,1-Dichloroethane ND 10 50 1,2,4-Trimethylbenzene ND 10 50 <br /> 1,2-bichloroethane ND 105 0 1,3,5-Tnrnethylbenzene ND 10 50 <br /> 1,1-Dichloroethene ND 10 5 0 Vinyl Acetate ° ND 5 0 25 <br /> cis-1,2-Dichlormthene ND 1 0 5 0 Vinyl Chlonde " ND 1 0 50 <br /> trans-l,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 10 50 <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluorornethane 98 <br /> I,1-Diehloropropene ND t 0 50 Toluene-d8 107 <br /> cis-1,3-Dichloropropene ND 1 0 5 0 4-Bromofluorobenzene 112 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (t) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />