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110 2nd Avenue South,4D7,Pacheco,CA 94553-5560
<br /> 4 WCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//www mccampbelI co m E-mail mam@mccampbell com
<br /> GEOSOLV, LLC Client Project ID Nunan/3ernigan Date Sampled 02/20-03/01/01
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Client P O Date Analyzed 03/05-03/08/01
<br /> Volatile Organics By GUMS
<br /> EPA method 8260
<br /> Lab ID 61521
<br /> Client ID MW-3 16-16
<br /> Matrix S
<br /> Reporting Limit Reporting Limn
<br /> Compound Concentration* WT 3 Compound Concentration* W S
<br /> Acetone ND<35 50 25 trans-1,3-Dichloropropene ND 10 50
<br /> Benzene ND 1 0 5 0 Ethylene dibromide ND 10 50
<br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND 10 5 0
<br /> Bromochloromethane ND 1 0 5 0 Hexachlorobutadiene ND 5 0 25
<br /> BromodiChlorOmethane ND 10 5 0 Iodomethane ND 10 50
<br /> Bromoform ND 1 0 5 Q Isopropylbenzene ND 10 5 0
<br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 50
<br /> n-Butyl benzene ND 10 5 0 Methyl butyl ketone ND 10 so
<br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chloride") ND 10 50
<br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND 20 10
<br /> Carbon Disulfide ND 1 0 5 0 Methyl isobutyl ketone 61 10 50
<br /> Carbon Tetrachloride ND 1 0 50 Methyl tent-Butyl Ether(MTBE) --- 10 5 0
<br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 50
<br /> Chloroethane ND 1 0 5 0 n-Propyl benzene ND 10 5 0
<br /> 2-Chloroethyl Vinyl Ether` ND 1 0 5 0 Styrene ND 10 5 0
<br /> Chloroform ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 50
<br /> 2-Chtorotoluene ND 1 0 5 0 Tetrachloroethene ND 10 5 0
<br /> 4-Chlorotoluene ND 1 0 5 0 Toluene 50 10 50
<br /> Dibromochloromethane ND 10 5 0 1,2,3-Trichlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 50 25
<br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 10 50
<br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnebloroethane ND 10 50
<br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 10 5 0
<br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 10 50
<br /> Dichlorodifluoromethane ND 10 50 1,2,3-Trichloropropane ND 10 50
<br /> 1,1-Dichloroethane ND 10 5 0 1,2,4-Trimethylbenzene ND 10 50
<br /> 1,2-Dichloroethane ND 10 50 1,3,5-Trimethylbenzene ND 10 50
<br /> I,1-Dichloroethene ND 1 0 50 Vinyl Acetate ') ND 50 25
<br /> cis-1 2-Dichloroethene ND 10 50 Vinyl Chlonde ° ND 10 50
<br /> trans-1,2-Dichloroethene ND 1 0 So Xylenes,total ND 10 50
<br /> 1,2-Dichloropropane ND 1 0 50 Comments
<br /> 1,3-Dichloropropane ND to 5 0 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 97
<br /> 1,l-Dic_hl oropropene i ND 1 0 5 0 Toluene-d8 105
<br /> cis-1,3-Dichloropropene IND 1 0 5 0 4-Bromofluorobenzene 84
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/5PLP extracts in ug/L
<br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is presen(, (i) liquid sample that contains greater than --5 vol %
<br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton, Lab Director
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