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110 2nd Avenue South,#D7,Pacheco,CA 94153-1560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmccampbelleo E-mail main@mccampbell com <br /> GEOSOLV, LLC Client Project 1D Nunan/Jermgan Date Sampled 02/20-03/01101 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Client P O Date Analyzed 03105-03108/01 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 61523 <br /> Client iD MW-3 2I -22 <br /> Matrix S <br /> Repmng Umrt Reponmg Lima <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone tip ND<100 50 25 trans-1,3-Dichloropropene ND<100 10 50 <br /> Benzene ND<100 10 50 Ethylene dibromide ND<100 10 50 <br /> Bromobenzene ND<100 1 0 50 Ethylbenzene 1300 10 50 <br /> Bromochloromethane ND<100 1 0 50 Hexachlorobutadiene ND<100 50 25 <br /> Bromodichloromethane ND<100 1 0 50 lodomethane ND<100 10 50 <br /> Bromoform ND<100 1 0 50 Isopropylbenzene 260 10 50 <br /> Bromomethane ND<100 1 0 50 p-Isopropyl toluene ND<100 10 50 <br /> n-Butyl benzene 630 1 0 50 Methyl butyl ketone ND<100 10 so <br /> sec-Butyl benzene 200 1 0 50 Methyiene Chloride"' ND<120 10 50 <br /> tert-Butyl benzene ND<100 1 0 50 Metbyl ethyl ketone ND<100 20 10 <br /> Carbon Disulfide ND<100 1 0 50 Methyl isobutyl ketones ND<100 10 50 <br /> Carbon Tetrachloride ND<100 1 0 50 Methyl tert-Bury!Ether(MTBE) --- 10 so <br /> Chlorobenzene ND<100 1 0 50 Naphthalene ND<100 50 50 <br /> Chloroethane ND<100 1 0 50 n-Propyi benzene 1000 10 5 0 <br /> 2-Chioroethyl Vinyl Ether` ND<100 1 0 5 0 Styrene W ND<100 10 50 <br /> Chloroform ND<100 1 0 5 0 1,1,1,2-Tetrachloroethane ND<100 1 0 5 0 <br /> Chloromethane ND<100 1 0 5 0 1,1,2,2-Tetrachloroethane ND<100 1 0 5 0 <br /> 2-Chlorotoluene ND<100 1 0 5 0 Tetrachloroethene ND<100 10 5 0 <br /> 4-Chlorotoluene ND<100 1 0 5 0 Toluene W NIK100 10 5 0 <br /> Dibromochloromethane ND<100 1 0 50 1,2,3-Trichlorobenzene ND<100 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND<100 2 0 10 1,2,4-Tnchlorobenzene ND<100 5 0 25 <br /> Dibromornethane ND<100 10 50 1,1,1-Tnchloroethane ND<100 to 5 0 <br /> 1,2-Dichlorobenzene ND<100 1 0 5 0 1,1,2-Tnchloroethane ND<100 10 5 0 <br /> 1 3-Dichlorobenzene ND<100 1 0 50 Tnchloroethene ND<100 10 50 <br /> 1 4-Dichlorobenzene ND<100 1 0 5 0 Trichlorofluoromethane ND<100 10 5 0 <br /> Dichlorodifluoromethane ND<100 1 0 50 1,2,3-Tnehloropropane ND<100 10 50 <br /> IJ-Dichloroethane ND<100 1 0 5 0 1,2,4-Tnmethylbenzene 2600 10 50 <br /> 1,2-Dichloroethane ND<100 1 0 5 0 1,3,5-Trimethylbenzene 1200 10 5 0 <br /> 1,1-Dichloroethene ND<100 1 0 5 0 Vinyl Acetate m ND<100 5 0 25 <br /> cis-1,2-Dichloroethene ND<100 1 0 5 0 Vinyl Chloride " ND<100 1 0 5 0 <br /> trans-l,2-Di chi omethene ND<100 1 0 5 0 Xylenes,total 1400 1 0 5 0 <br /> 1,2-Dichloropropane ND<100 10 50 Comments <br /> 1,3-Dichloropropane ND<100 1 0 5 0 Surrogate Recoveries{%) <br /> 2,2-Dichloropropane ND<100 1 0 5 0 DlbromoflUoramethane 91 <br /> 1,1-Dichloropropene ND<100 10 50 Toluene-d8 102 <br /> cis-1,3-Dichloropropene ND<100 1 0 5 0 4-Bromofluorobenzene 94 <br /> water and vapor samples are reported in ugll.,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> 1 ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2 <br /> pentanone or isopropy I acetone, (h) lighter than water immiscible sheen is present, (t)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to bigh organic content (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />