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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http//Wwwmccampbellcom E-mail main@mccampbell com <br /> GEOSOLV, LLC Client Project ID Nunan/3ernigan Date Sampled 02120-03/01/01 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Client P O Date Analyzed 03/05-03/08/01 <br /> 1Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 61537 <br /> Client ID MW-3 86-86 <br /> Matrix S <br /> Reporting L�ml[ Reporting Lima <br /> Compound Concentration* � S Compound Concentration* W S <br /> 1 Acetone ai ND<35 50 25 trans-1,3-Dichloropropene ND to 50 <br /> Benzene ND 10 50 Ethylene dibromde ND 10 50 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 10 50 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 10 5 0 <br /> Bromoform ND 1 0 5 0 lsopropylhenzene ND 10 5 0 <br /> Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 10 50 <br />' n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 10 50 <br /> see-Butyl benzene ND 1 0 5 0 Methylene Chloride"' ND 10 50 <br /> tent-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 1 0 5 0 Methyl isobutyl ketone a ND 10 50 <br /> Carbon Temchlonde ND 1 0 5 6 Methyl tert-Butyl Ether(MTBE) --- 10 50 <br /> Chlorobenzene ND 1 0 5 0 Naphthalene ND 50 so <br /> Chloroethane ND 1 0 5 0 n-Propyl benzene ND 10 50 <br /> 2 Chloroethyl Vinyl Ether` ND 1 0 5 0 Styrene ND 1 0 50 <br />' Chloroform ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 1 0 5 0 <br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 10 5 0 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 1 0 5 0 <br /> 4-Chlorotoluene ND 1 0 5 0 Toluene 43 1 0 5 0 <br />' Dibromochloromethane ND 1 0 5 0 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Trichlorobenzene ND 5 0 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Trichloroethane ND 10 50 <br /> 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Trichloroethane ND 10 5 0 <br /> 1,3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 10 50 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Tnchlorofluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Trichloropropane ND to 5 0 <br /> IJ-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 5 0 <br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Tnmethylbenzene ND 10 5 0 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate ro ND 50 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride ° ND 10 50 <br /> trans-1,2-Dichloroethene ND 1 0 50 Xylenes,total ND 10 50 <br /> 1,2-Dichloropropane ND 1 0 5 0 Comments <br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 98 <br /> 1,1-Dichloropropene ND 1 0 5 0 Toluene-d8 103 <br /> cis-1,3-Di chloropropene ND 1 0 5 0 1 4-Bromofluorobenzene 89 <br /> water and vapor samples are reported in ug/L soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-cbloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, 1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethane,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />