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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> htto//www mccampbell corn E-mail main@mccampbell corn
<br /> GEOSOLV, LLC Client Project ID Nunan/Jernigan Date Sampled 02/20-03/01/01
<br /> 643 Oregon Street Date Received 03/01/01
<br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01
<br /> Cltent P O Date Analyzed 03/05-03/08/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 61533
<br /> Client ID MW-3 80"'-81
<br /> Matrix J S
<br /> Reporting Limit Reporting Limit
<br /> Compound Concentration* Reporting
<br /> S Compound Concentration* W S
<br /> Acetone rot ND<35 50 25 trans-1,3-Dtchloropropene ND 10 50
<br /> Benzene ND 1 0 5 0 Ethylene dibromide ND 1 0 5 0
<br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 1 0 5 0
<br /> Bromochloromethane ND 1 0 5 0 Hexachlorobutadiene ND 5 0 25
<br /> Bromodichloromethane ND 1 0 5 0 lodomethane ND 10 1 50
<br /> Bromoform ND 1 0 50 Isopropylbenzene ND 1 0 5 0
<br /> Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 10 5 0
<br /> 1 n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 10 5 0
<br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chloride` ND 10 50
<br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketene a ND 10 5 0
<br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) --- 10 5 0
<br /> Chlorobenzene ND 1 0 5 0 Naphthalene ND 50 50
<br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 1 0 5 0
<br /> 2-Chloroethyl Vinyl Ether"' ND 1 0 50 Styrene ND 1 0 5 0
<br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 5 0
<br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 10 5 0
<br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethane ND 1 0 50
<br /> 4-Chlorotoluene ND 1 0 50 Toluene ND to 5 0
<br /> Dibrornochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chlompropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25
<br /> Dibromomethane ND to 5 0 1,1,1-Trichloroethane ND 10 5 0
<br /> 1,2-Dichloroben4ene ND 10 5 0 1,I,2-Tnchloroethane ND 10 50
<br /> 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND 10 50
<br /> 1,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 1 0 5 0
<br /> Dichloroditluommethane ND 10 50 1,2,3-Tnehloropropane ND 10 50
<br /> 1,1-Dichloroethane ND 1 0 50 1,2,4-Tnmethylbenzene ND 10 50
<br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Tnmethylbenzene ND 1 0 5 0
<br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate m ND 50 25
<br /> cis-1,2 Dichloroethene ND 1 0 5 0 Vinyl Chloride in) ND 10 5 0
<br /> trans-1,2-Dichloroethene ND 1 0 50 Xylenes,total ND 10 5 0
<br /> 1,2-Dichloropropane ND to 50 Comments
<br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 10 50 Dibromofluoromethane 96
<br /> I,1-Dtchloropropene ND 10 50 Toluene-d8 102
<br /> cis-1,3 Dichloropropene ND 10 50 4-Bromofluorobenzene 94
<br /> `water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c)(2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
<br /> f
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