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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 WCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> littp//wvw mccampbell com E-mail main@mccampbell com <br /> GEOSOLV,LLC Client Project ID Nunan/Jernigan Date Sampled 02120-03101/01 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Lent <br /> PO Date Analyzed 03105-03/08/01 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 61514 61516 61518 61519 <br /> MW-260"z- MW-2 83 - MW-2 88 - MW-298,111- Reporting Limit <br /> Client ID 61 84 89 99 <br /> Matrix S S S S S W <br /> Compound Concentration* ug/kg uglL <br /> Di-isopropyl Ether(DIPS) ND ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 10 <br /> Cert-Butanol ND ND ND ND 25 50 <br /> Methanol ND ND ND ND 1000 200 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromotluoromethane 98 98 98 97 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in uglL <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br />' (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,(1)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />