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110 2nd Avenue South,#D7,Pacheco CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925- 798-1622 <br /> http//www mccampbell com E-mail main@mccampbell Com <br /> GEOSOLV, LLC Client Project ID Nunan/Jernlgan Date Sampled 02/20-03/01101 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Client P O Date Analyzed 03/05-03108/01 <br /> 7 Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br /> Lab ID 61520 61521 61523 61524 <br /> MW-3 10 - MW-3 16- MW-3 21 - MW-3 23 _ Reporting Limit <br /> Client ID 11 1614 22 24 <br /> Matrix S S S S S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(RIPE) ND ND ND<100 ND 50 1 0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND<100 ND 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND<100 ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND<100 ND 50 1 0 <br /> tert-Butanol ND ND ND<500 ND 25 50 <br /> Methanol ND ND ND<20,000 ND 1000 200 <br /> Ethanol ND ND ND<5000 ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromolluoromethane 97 97 91 96 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment 6)sample diluted due to <br /> high organic content <br /> i <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> 1 <br />