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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> J4 1 http//www mccampbell coin E-matt main@mccampbell com <br /> GEOSOLV,LLC Client Protect ID Nunan/Jernigan Date Sampled 02/20-03/01/01 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Client P O Date Analyzed 03/05-03/08/01 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 61525 61526 61528 61530 <br />' MW-3 30112- MW-3 36- —M—W--3-45=- W <br /> - M -3 60 - Reporting Limit <br /> Client ID 31 36 1/2 46 61 <br /> Matrix S S S S S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND<100 ND ND ND 50 1 0 <br />' Ethyl tert-Butyl Ether(ETRE) ND<100 ND ND ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND<100 ND ND ND 50 10 <br /> tent-Amyl Methyl Ether(TAME) ND<]00 ND ND ND 50 10 <br /> tert-Butanol ND<500 ND ND ND 25 50 <br />' Methanol ND<20,000 ND ND ND 1000 200 <br /> Ethanol ND<5000 ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br />' DibromoIIuoromethane 90 90 97 96 <br />' Comments ] <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 J4—Edward Hamilton,Lab Director <br />