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011pha Analytical, Inc. 0 <br /> 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431-5778 <br /> (775) 355-1044 • (775) 355-0406 FAX • 1-800-283-1183 <br /> Date: Work Order: <br /> 31-Oct-06 QC Summary Report 06102306 <br /> Method Blank Type MBLK Test Code: EPA Method SW8015B <br /> File ID: 06102410.D Batch ID: MS15S5926B Analysis Date: 10/24/2006 12:11 <br /> Sample ID: MBLK MS15S5926B Units : pg/Kg Run ID:MSD_15_061024B Prep Date: 10/24/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-P (GRO) ND 1000 <br /> Surr: 1,2-Dichloroethane-d4 215 200 107 68 119 <br /> Surr:Toluene-d8 198 200 99 84 116 <br /> Surr:4-Bromofluorobenzene 184 200 92 72 118 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8015B <br /> File ID: 06102409.D Batch ID: MS15S5926B Analysis Date: 10/24/2006 11:49 <br /> Sample ID: GLCS MS1535926B Units : pg/Kg Run ID:MSD_15_061024B Prep Date: 10/24/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-P (GRO) 16200 2000 16000 101 60 153 <br /> Surr: 1,2-Dichloroethane-d4 436 400 109 68 119 <br /> Surr:Toluene-d8 384 400 96 84 116 <br /> Surr:4-Bromofluorobenzene 377 400 94 72 118 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8015B <br /> File ID: 06102413.D Batch ID: MS15S5926B Analysis Date: 10/24/2006 13:19 <br /> Sample ID: 06102306-02AGS Units : pg/Kg Run ID:MSD_15_061024B Prep Date: 10/24/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qua] <br /> TPH-P (GRO) 14800 2000 16000 0 92 8 177 <br /> Surr: 1,2-Dichloroethane-d4 450 400 112 68 119 <br /> Surr:Toluene-d8 379 400 95 84 116 <br /> Surr:4-Bromofluorobenzene 367 400 92 72 118 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8015B <br /> File ID: 06102414.11) Batch ID: MS15S5926B Analysis Date: 10/24/2006 13:41 <br /> Sample ID: 06102306-02AGSD Units : pg/Kg Run ID:MSD_15_061024B Prep Date: 10/24/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-P (GRO) 15000 2000 16000 0 94 8 177 14790 1.5(45) <br /> Surr: 1,2-Dichloroethane-d4 436 400 109 68 119 <br /> Surr:Toluene-d8 380 400 95 84 116 <br /> Sum 4-Bromofluorobenzene 370 400 93 72 118 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting proposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> Reported in micrograms per kilogram,per client request. <br />