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011pha Analytical, Ince r <br /> 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431-5778 <br /> (775) 355-1044 • (775) 355-0406 FAX• 1-800-283-1183 <br /> Date: <br /> ork Order: <br /> 31-Oct-06 QC Su=ary Report 0610230066 <br /> 06102 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: 06102410.D Batch ID: MS15S5926A Analysis Date: 10/24/200612:11 <br /> Sample ID: MBLK MS15S5926A Units : pg/Kg Run ID:MSD_15_061024B Prep Date: 10/24/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol (TBA) ND 500 <br /> Methyl tert-butyl ether(MTBE) ND 5 <br /> Di-isopropyl Ether(DIPE) ND 20 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 20 <br /> Benzene ND 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 20 <br /> Toluene ND 5 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene ND 5 <br /> o-Xylene ND 5 <br /> Surr: 1,2-Dichloroethane-d4 215 200 107 68 119 <br /> Surr:Toluene-d8 198 200 99 84 116 <br /> Surr:4-Bromofluorobenzene 184 200 92 72 118 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID:06102408.13 Batch ID: MS15S5926A Analysis Date: 10/24/2006 11:26 <br /> Sample ID: LCS MS15S5926A Units : pg/Kg Run ID:MSD_15_061024B Prep Date: 10/24/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 466 10 400 116 58 147 <br /> Toluene 413 10 400 103 58 148 <br /> Ethylbenzene 418 10 400 105 59 151 <br /> m,p-Xylene 448 10 400 112 60 155 <br /> o-Xylene 460 10 400 115 62 155 <br /> Surr: 1,2-Dichloroethane-d4 443 400 111 68 119 <br /> Surr:Toluene-d8 372 400 93 84 116 <br /> Surr:4-Bromofluorobenzene 380 400 95 72 118 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> File ID: 06102411.D Batch ID: MS15S5926A Analysis Date: 10/24/2006 12:34 <br /> Sample ID: 06102306-02AMS Units : pg/Kg Run ID:MSD_15_061024B Prep Date: 10/24/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 438 10 400 0 109 30 151 <br /> Toluene 391 10 400 0 98 25 159 <br /> Ethylbenzene 397 10 400 0 99 27 161 <br /> m,p-Xylene 423 10 400 0 106 22 170 <br /> o-Xylene 432 10 400 0 108 22 171 <br /> Surr: 1,2-Dichloroethane-d4 449 400 112 68 119 <br /> Surr:Toluene-d8 370 400 92 84 116 <br /> Surr:4-Bromofluorobenzene 376 400 94 72 118 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> File ID: 06102412.13 Batch ID: MS15S5926A Analysis Date: 10/24/2006 12:56 <br /> Sample ID: 06102306-02AMSD Units : pg/Kg Run ID:MSD_15_061024B Prep Date: 10/24/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 432 10 400 0 108 30 151 437.6 1.3(37) <br /> Toluene 383 10 400 0 96 25 159 390.5 1.9(40) <br /> Ethylbenzene 385 10 400 0 96 27 161 397.2 3.0(39) <br /> m,p-Xylene 408 10 400 0 102 22 170 423.3 3.6(40) <br /> o-Xylene 423 10 400 0 106 22 171 432 2.2(41) <br /> Surr: 1,2-Dichloroethane-d4 444 400 111 68 119 <br /> Surr:Toluene-d8 367 400 92 84 116 <br /> Surr:4-Bromofluorobenzene 377 400 94 72 118 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br />