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QC Sample Results C <br /> Client: Dudek&Associates TestAmerica Job ID: 440-223576-1 <br /> Project/Site: Kearney KPF SDG: Stockton, CA <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCS 440-509443/3 Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 509443 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> 1,1-Dichloropropene 25.0 27.9 ug/L 112 70-130 <br /> 1,2-Dichlorobenzene 25.0 27.0 ug/L 108 70-130 <br /> 1,2-Dichloroethane 25.0 32.9 ug/L 132 57-138 <br /> 1,2-Dichloropropane 25.0 28.8 ug/L 115 67-130 <br /> 1,3-Dichlorobenzene 25.0 26.4 ug/L 106 70-130 <br /> 1,4-Dichlorobenzene 25.0 27.0 ug/L 108 70-130 <br /> Bromodichloromethane 25.0 33.2 ug/L 133 70-132 <br /> Bromoform 25.0 30.4 ug/L 122 60-148 <br /> Bromomethane 25.0 26.9 ug/L 108 64-139 m <br /> Carbon tetrachloride 25.0 32.7 ug/L 131 60-150 <br /> Chlorobenzene 25.0 27.2 ug/L 109 70-130 <br /> Chloroethane 25.0 26.5 ug/L 106 64-135 <br /> Chloroform 25.0 31.4 ug/L 126 70-130 <br /> Chloromethane 25.0 25.5 ug/L 102 47-140 <br /> cis-1,2-Dichloroethene 25.0 28.6 ug/L 114 70-133 ❑ <br /> cis-1,3-Dichloropropene 25.0 30.5 ug/L 122 70-133 <br /> Dibromochloromethane 25.0 31.5 ug/L 126 69-145 <br /> Dichlorodifluoromethane 25.0 25.0 ug/L 100 29-150 <br /> Methylene Chloride 25.0 27.4 ug/L 109 52-130 <br /> Tetrachloroethene 25.0 26.9 ug/L 108 70-130 <br /> trans-1,2-Dichloroethene 25.0 28.0 ug/L 112 70-130 <br /> trans-1,3-Dichloropropene 25.0 29.9 ug/L 120 70-132 <br /> Trichloroethene 25.0 28.2 ug/L 113 70-130 <br /> Trichlorofluoromethane 25.0 30.9 ug/L 124 60-150 <br /> Vinyl chloride 25.0 25.1 ug/L 100 59-133 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene(Surr) 99 80-120 <br /> Dibromofluoromethane(Surr) 112 76-132 <br /> Toluene-d8(Surr) 106 80-128 <br /> Lab Sample ID: 440-223576-11 MS Client Sample ID: KEW-3U <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 509443 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,1,1,2-Tetrachloroethane ND 25.0 28.9 ug/L 116 60-149 <br /> 1,1,1-Trichloroethane ND 25.0 32.2 ug/L 129 70-130 <br /> 1,1,2,2-Tetrachloroethane ND 25.0 23.6 ug/L 94 63-130 <br /> 1,1,2-Trichloroethane ND 25.0 26.1 ug/L 104 70-130 <br /> 1,1-Dichloroethane ND 25.0 28.1 ug/L 112 65-130 <br /> 1,1-Dichloroethene 6.4 25.0 33.3 ug/L 108 70-130 <br /> 1,1-Dichloropropene ND 25.0 27.5 ug/L 110 64-130 <br /> 1,2-Dichlorobenzene ND 25.0 26.4 ug/L 106 70-130 <br /> 1,2-Dichloroethane ND 25.0 32.8 ug/L 131 56-146 <br /> 1,2-Dichloropropane ND 25.0 27.7 ug/L 111 69-130 <br /> 1,3-Dichlorobenzene ND 25.0 25.7 ug/L 103 70-130 <br /> 1,4-Dichlorobenzene ND 25.0 25.9 ug/L 104 70-130 <br /> TestAmerica Irvine <br /> Page 25 of 34 11/15/2018 <br />