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QC Sample Results C <br /> Client: Dudek&Associates TestAmerica Job ID: 440-223576-1 <br /> Project/Site: Kearney KPF SDG: Stockton, CA <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: 440-223576-11 MS Client Sample ID: KEW-3U <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 509443 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Bromodichloromethane ND 25.0 31.6 ug/L 127 70-138 <br /> Bromoform ND 25.0 28.5 ug/L 114 59-150 <br /> Bromomethane ND 25.0 26.5 ug/L 106 62-131 <br /> Carbon tetrachloride ND 25.0 32.8 ug/L 131 60-150 <br /> Chlorobenzene ND 25.0 25.5 ug/L 102 70-130 <br /> Chloroethane ND 25.0 25.8 ug/L 103 68-130 <br /> Chloroform ND 25.0 30.2 ug/L 121 70-130 <br /> Chloromethane ND 25.0 24.2 ug/L 97 39-144 <br /> cis-1,2-Dichloroethene ND 25.0 27.7 ug/L 111 70-130 m <br /> cis-1,3-Dichloropropene ND 25.0 28.8 ug/L 115 70-133 <br /> Dibromochloromethane ND 25.0 28.7 ug/L 115 70-148 <br /> Dichlorodifluoromethane ND 25.0 25.0 ug/L 100 25-142 <br /> Methylene Chloride ND 25.0 23.4 ug/L 94 52-130 <br /> Tetrachloroethene 3.2 25.0 28.3 ug/L 101 70-137 <br /> trans-1,2-Dichloroethene ND 25.0 27.2 ug/L 109 70-130 ❑ <br /> trans-1,3-Dichloropropene ND 25.0 26.9 ug/L 108 70-138 <br /> Trichloroethene 9.2 25.0 36.9 ug/L 111 70-130 <br /> Trichlorofluoromethane ND 25.0 31.1 ug/L 125 60-150 <br /> Vinyl chloride ND 25.0 24.6 ug/L 98 50-137 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene(Surr) 97 80-120 <br /> Dibromofluoromethane(Surr) 113 76-132 <br /> Toluene-d8(Surr) 100 80-128 <br /> Lab Sample ID: 440-223576-11 MSD Client Sample ID: KEW-3U <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 509443 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1,1,2-Tetrachloroethane ND 25.0 28.3 ug/L 113 60-149 2 20 <br /> 1,1,1-Trichloroethane ND 25.0 30.8 ug/L 123 70-130 4 20 <br /> 1,1,2,2-Tetrachloroethane ND 25.0 23.4 ug/L 93 63-130 1 30 <br /> 1,1,2-Trichloroethane ND 25.0 25.9 ug/L 104 70-130 1 25 <br /> 1,1-Dichloroethane ND 25.0 27.5 ug/L 110 65-130 2 20 <br /> 1,1-Dichloroethene 6.4 25.0 30.9 ug/L 98 70-130 8 20 <br /> 1,1-Dichloropropene ND 25.0 26.5 ug/L 106 64-130 4 20 <br /> 1,2-Dichlorobenzene ND 25.0 25.4 ug/L 102 70-130 4 20 <br /> 1,2-Dichloroethane ND 25.0 32.3 ug/L 129 56-146 1 20 <br /> 1,2-Dichloropropane ND 25.0 26.6 ug/L 107 69-130 4 20 <br /> 1,3-Dichlorobenzene ND 25.0 24.8 ug/L 99 70-130 4 20 <br /> 1,4-Dichlorobenzene ND 25.0 25.0 ug/L 100 70-130 4 20 <br /> Bromodichloromethane ND 25.0 30.5 ug/L 122 70-138 4 20 <br /> Bromoform ND 25.0 27.6 ug/L 110 59-150 3 25 <br /> Bromomethane ND 25.0 26.0 ug/L 104 62-131 2 25 <br /> Carbon tetrachloride ND 25.0 30.2 ug/L 121 60-150 8 25 <br /> Chlorobenzene ND 25.0 25.0 ug/L 100 70-130 2 20 <br /> Chloroethane ND 25.0 24.9 ug/L 99 68-130 4 25 <br /> TestAmerica Irvine <br /> Page 26 of 34 11/15/2018 <br />