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QC Sample Results C <br /> Client: Dudek&Associates TestAmerica Job ID: 440-223576-1 <br /> Project/Site: Kearney KPF SDG: Stockton, CA <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: 440-223576-11 MSD Client Sample ID: KEW-3U <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 509443 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Chloroform ND 25.0 29.4 ug/L 117 70-130 3 20 <br /> Chloromethane ND 25.0 25.1 ug/L 100 39-144 4 25 <br /> cis-1,2-Dichloroethene ND 25.0 28.0 ug/L 112 70-130 1 20 <br /> cis-1,3-Dichloropropene ND 25.0 27.8 ug/L 111 70-133 4 20 <br /> Dibromochloromethane ND 25.0 28.3 ug/L 113 70-148 2 25 <br /> Dichlorodifluoromethane ND 25.0 23.6 ug/L 94 25-142 6 30 <br /> Methylene Chloride ND 25.0 23.1 ug/L 92 52-130 2 20 <br /> Tetrachloroethene 3.2 25.0 26.7 ug/L 94 70-137 6 20 <br /> trans-1,2-Dichloroethene ND 25.0 27.2 ug/L 109 70-130 0 20 m <br /> trans-l,3-Dichloropropene ND 25.0 27.0 ug/L 108 70-138 0 25 <br /> Trichloroethene 9.2 25.0 34.5 ug/L 101 70-130 7 20 <br /> Trichlorofluoromethane ND 25.0 29.0 ug/L 116 60-150 7 25 <br /> Vinyl chloride ND 25.0 24.3 ug/L 97 50-137 1 30 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits F14-Bromofluorobenzene(Surr) 95 80-120 <br /> Dibromofluoromethane(Surr) 111 76-132 <br /> Toluene-d8(Surr) 97 80-128 <br /> Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) <br /> F-Lab Sample ID: MB 440-509527/1-A Client Sample ID: Method Blank <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 509815 Prep Batch: 509527 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> 1,4-Dioxane ND 1.0 0.10 ug/L 11/06/1810:47 11/07/1815:32 1 <br /> MB MB <br /> Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac <br /> 1,4-Dioxane-d8(Surr) 67 27-120 11/06/18 10:47 11/07/18 15:32 1 <br /> Lab Sample ID: LCS 440-509527/3-A Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 509815 Prep Batch: 509527 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> 1,4-Dioxane 2.00 1.00 ug/L 50 36-120 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> 1,4-Dioxane-d8(Surr) 48 27-120 <br /> Lab Sample ID: 440-223576-11 MS Client Sample ID: KEW-3U <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 509815 Prep Batch: 509527 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,4-Dioxane 2.8 1.99 4.04 ug/L 64 10-150 <br /> TestAmerica Irvine <br /> Page 27 of 34 11/15/2018 <br />