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j <br /> Spargero Analytical Laboratory Division <br /> { <br /> Tbichnology,.. Mobile Laboratory Division <br /> Scientific Division <br /> With Automation in Mind I <br /> 1. <br /> i Modified EPA Method 8260 GCMS <br /> OXYGENATES <br /> Method Blank <br /> Attention: Mr. Tom Landwehr <br /> Date Sampled: Oct 19, 1999 <br /> Apex Envirotech Date Received: Oct 20, 1999 <br /> 7844 Madison Ave. Date Analyzed: Oct 20, 1999 <br /> Fair Oaks, CA 95628 Invoice# 11614OCT99 <br /> Project#: ERA02.004 Project Name: Moore Petroleum <br /> Bulk Plant <br /> I Client ID: Method Blank LAB ID: QC-BATCH <br /> Matrix: Soil Dilution: 1: 1 <br /> k <br /> Reporting <br /> Compound Name Concentration Limit Units <br /> 1.) Tertiary butanol ND 10 <br /> ug/kg <br /> 2.) Methyl-tert-butyl-ether(MTBE) ND 2.0 ug/kg <br /> I <br /> 3.) Di-isopropyl ether ND 5.0 ug/kg <br /> 4.) Ethyl tertiary butyl ether ND. 5.0 ug/kg <br /> f 5.) Tertiary amyl methyl ether ND 5.0 <br /> ug/kg <br /> Surrogate % Recovery of 1,2-dichloroethane-d4 = 97% <br /> PPI)=parts per billion=uglkg=micrograms per kilogram <br /> ppm=parts per million=mg/kg=milligrams per kilogram <br /> ND=Not Defected. Compound(s)may be present at concentrations below the reporting limit. <br /> . i <br /> r <br /> F <br /> Oct 20, 1999 <br /> R. L-James, Principal Chemist Date Reported <br /> f SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> Oxygenate(S).xis <br /> 3050 Fite Circle Suite 112 • Sacramento, California 95827• (916) 362-8947 0 FAX(9f6)'362-0947 <br />