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i <br /> I <br /> SpargerAnalytical Laboratory Division <br /> 0 <br /> Mobile Laboratory Division `. <br /> Technologyinc. Scientific Division <br /> I <br /> With Automation in Mind <br /> EPA Method 8260 GCMS Analysis Report <br /> Laboratory Control Spike (LCS) and Laboratory Control Spike Duplicate (LCSD) : <br /> Attention: Mr. Tom Landwehr Date Sampled: Oct 19, 1999 k <br /> Apex Envirotech Date Received: Oct 20, 1999 <br /> 7844 Madison Ave. Date Analyzed: Oct 20, 1999 <br /> Fair Oaks, CA 95628 Invoice#: 11614OCT99 <br /> - I <br /> Project#: ERA02.004 Project Name: Moore Petroleum <br /> f Bulk Plant <br /> Client ID: LCS/LCSD LAB ID: QC-BATCH ! <br /> Matrix: Soil Dilution: 1: 1 <br /> Units = (ug/kg) <br /> Sample Spike (ppb) Spike Dup. Spike Dup, QC Limits <br /> Compound Conc Added Result Result %'Rec % Rec RPD RPD % Rec <br /> Tertiary butanol ND 50 56 59 112% 118% 5% 22 , 59-172 J <br /> Methyl-tert-butyl-ether(MTBE) ND 50 47 48 94% 96% 2% <br /> 24 62-142 <br /> Di-isopropyl ether ND 50 39 39 78% 78% 0% 21 60-137 <br /> Ethyl tertiary butyl ether ND 50 42 42 84% 84% 0% 21 59-139 <br /> Tertiary amyl methyl ether ND 50 45 45 90% 90% 0% 21 66-133 <br /> ppb=parts per billion=uglkg=micrograms per kilogram _ <br /> ppm=parts per million=uglg=micrograms per gram <br /> ND=Not Detected. Ccmpound(s)may be present at concentrations below the detection limit. <br /> I <br /> Oct 20, 1999 r <br /> R. L.James, Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> OEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> Oxygen ate(S).xIs <br /> 3050 Fite Circle, Suite 112 • Sacramento, California 95827 7• (946) 362-8947 • FAX(946) 362-0947 <br />