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1 <br /> Sparger 0 <br /> Analytical Laboratory Division <br /> TechnologyInc. Mobile Laboratory Division <br /> With Automation in MindScientific Division <br /> EPA Method 8260 GCMS Analysis Report <br /> Matrix Spike (MS) and Matrix Spike Duplicate (MSD) <br /> Attention: Mr. Tom Landwehr Date Sampled: Oct 19, 1999 <br /> Apex Envirotech Date Received: Oct 20, 1999 <br /> 7844 Madison Ave. Date Analyzed: Oct 20, 1999 <br /> Fair Oaks, CA 95628 Invoice#: 11614OCT99 <br /> Project#: ERA02.004' Project Name: Moore Petroleum <br /> Bulk Plant <br /> Client ID: x MS/MSD LAB ID: 11614-001MSIMSD <br /> Matrix: Soil Dilution: 1: 1 <br /> Units =(uglkg) <br /> Sample Spike (ppb) Spike Dup. Spike Dup. i Limits <br /> rr Compound Conc Added Result Result % Rec % Rec RPD RPD % Rec <br /> Ir <br /> f � <br /> Tertiary butanol ND 50 60 60 120% 120% 0% 22 59-172. <br /> f. Methyl-tert-butyl-ether(MTBE) 3.1 50 49 49 92% 92% 0% 24 62-142 <br /> Di-isopropyl ether ND 50 36 37 72% 74% 3% 21 60-137 <br /> Ethyl tertiary butyl ether ND 50 41 42 82% 84% 2% 21 59-139 <br /> Tertiary amyl methyl ether ND 50 44 45 88% 90% 2% 21 66-133 <br /> k ppb=parts per billion=uglkg=micrograms per kilogram <br /> ppm=parts per million=uglg=micrograms per gram <br /> } <br /> ND=Not Detected. Compounds)may be present at concentrations below the detection limit <br /> 1 <br /> Oct 20, 1999 <br /> �.L.James,Principal Chemist Date Reported <br /> i <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA _ <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> Oxygenate(S).xis' <br /> 3050 Fite Circle, Suite 112 • Sacramento, Colifomio 95827 + (916).362-8947 is FAX(946) 362-0947 <br />