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BSKANALYTICAL <br /> LABORATORIES <br /> Tony Martin Certificate of Analysis <br /> j Kleinfelder Inc ELAP Certificate#1180 <br /> 2825 East Myrtle Street Report Issue Date: 05/24/2002 <br /> j Stockton, CA 95205-4794 <br /> BSK Submission#: 2002050830 <br /> BSK Sample ID#: 207754 <br /> Project ID: Disco Project Desc: 2nd Qtr.G.W.Mon. <br /> Submission Cotnments: <br /> Sample Type: Liquid Date Sampled: 05/13/2002 <br /> Sample Description: MW-13 Time Sampled: 0942 <br /> Sample Comments: Date Received: 05/15/2002 <br /> Organics Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date . Date <br /> TPH as Gasoline EPA 8015(M) ND Itg/L 50 1 50 05/20/2002 05/20/2002 <br /> Benzene EPA 8020 ND gg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> Ethylbenzene EPA 8020 ND µg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> Toluene EPA 8020 ND µg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> Total Xylenes EPA 8020 ND µg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> i,2-Dibromoethane EPA 8260 ND µg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> 1,2-Dichloroethane EPA 8260 ND µg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> Di-isopropyl Ether EPA 8260 ND µg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> Ethyl t-Butyi Ether EPA 8260 ND }tg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> Methyl-t-Butyl Ether EPA 8260 ND µg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> t-Amyl Methyl Ether EPA 8260 ND gg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> tert-Butyl Alcohol EPA 8260 ND µg/L 50 1 50 05/20/2002 05/20/2002 <br /> Surrogate <br /> ----------------------------- .................---.......----------------------------------------------------------------------------------------------------------------- <br /> I Fluorobenzene EPA 8020 91.3 %Rec - 1 N/A 05/20/2002 05/20/2002 <br /> Toluene-d8 EPA 8260 103 %Rec - 1 N/A 05/20/2002 05/20/2002 <br /> i <br /> mg/L:Milligrams/Liter(ppm) PQL: Practical Quantitation Limit H:Analyzed outside of hold time <br /> mg/Kg: Milligrams/Kilogram(ppm) DLR: Detection Limit for Reporting P: Preliminary result <br /> gg/L: Micrograms/Liter(ppb) :PQL x Dilution S:Suspect result. See Cover Letter for comments. <br /> µg/Kg: Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. <br /> %Rec: Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: 1111111IIIAIIIIIIIIIIIIIIIIIIII1III11IIII1I1IIN1111111111111111111IIIA///III Pagel of7 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />