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BSKANALYTICAL <br /> LABORATORIES <br /> Tony Martin Certificate of Analysis <br /> Kleinfelder Inc ELAP Certificate #1180 <br /> 2825 East Myrtle Street Report Issue Date: 05/24/2002 <br /> Stockton, CA 95205-4794 <br /> BSK Submission#: 2002050830 <br /> BSK Sample TD #: 207755 <br /> Project ID: Disco Project Dese: 2nd Qtr.G.W.Mon. <br /> Submission Comments: <br /> Sample Type: Liquid Date Sampled: 05/13/2002 <br /> Sample Description: MW-12 Time Sampled: 1016 <br /> Sample Comments: Date Received: 05/15/2002 <br /> Organics Piep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) ND µg/L 50 1 50 05/20/2002 05/20/2002 <br /> Benzene EPA 8020 ND lig/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> Ethylbenzene EPA 8020 ND µg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> Toluene EPA 8020 ND µg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> Total Xylenes EPA 8020 ND µg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> 1,2-Dibromoethane EPA 8260 ND µg1L 5.0 1 5 05/20/2002 05/20/2002 <br /> ,2-Dichloroethane EPA 8260 ND lig/L 5.0 1 5.0 05/20/2002 05/20/2002 <br /> Di-isopropyl Ether EPA 8260 ND µg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> ! Ethyl t-Butyl Ether EPA 8260 ND µg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> Methyl-t-Butyl Ether GPA 8260 ND lig/L 5.0 1 5 05/20/2002 05/20/2002 <br /> t-Amyl Methyl Ether SPA 8260 ND gg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> tert-Butyl Alcohol EPA 8260 ND gg/L 50 1 50 05/20/2002 05/20/2002 <br /> Surrogate <br /> •------------------------•-----..-----------------------------------------------.....------------------------------....------------- <br /> Fluorobenzene EPA 8020 110.4 /o Rec - 1 N/A 05/20/2002 05/20/2002 <br /> Toluene-d8 EPA 8260 102.9 %Rec - 1 N/A 05/20/2002 05/20/2002 <br /> i <br /> mg/L: Milligrams/Liter(ppm) PQL: Practical Quantitation Limit H:Analyzed outside of hold time <br /> mg/Kg: Milligrams/Kilogram(ppm) DLR: Detection Limit for Reporting P: Preliminary result <br /> µg/L: Micrograms/Liter(ppb) : PQL x Dilution S: Suspect result. See Cover Letter for comments. <br /> µg/Kg: Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Anaiysis performed by External laboratory. <br /> %Rec: Percent Recovered(surrogates) See Extemal Laboratory Report attachments. <br /> } Report Authentication Code: 1111111 IN IN 1111111111111111111111111111111111111 HIM III IN 111111111111 Page 2 of 7 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />