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BSKANALYTICAL <br /> LABORATORIES <br /> Tony Martin Certificate of Analysis <br /> Kleinfelder Inc ELAP Certificate#1180 <br /> 2825 East Myrtle Street Report Issue Date: 05/24/2002 <br /> Stockton, CA 95205-4794 <br /> BSK Submission#: 2002050830 <br /> BSK Sample ID#: 207758 <br /> Project ID: Disco Project Desc: 2nd Qtr.G.W.Mon. <br /> Submission Comments: <br /> Sample Type: Liquid Date Sampled: 05/13/2002 <br /> Sample Description: MW-11D Time Sampled: 1340 <br /> Sample Comments: Date Received: 05/15/2002 <br /> Organics <br /> Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) ND gg/L 50 l 50 05/20/2002 05/20/2002 <br /> Benzene EPA 8020 ND µg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> Ethylbenzene EPA 8020 ND }tg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> Toluene EPA 8020 ND Ag/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> f Total Xylenes EPA 8020 ND gg/L 0.3 l 0.3 05/20/2002 05/20/2002 <br /> 1,2-Dibromoethane EPA 8260 ND }tg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> 1,2-Dichloroethane EPA 8260 ND AglL 5.0 1 5 05/20/2002 05/20/2002 <br /> Di-isopropyl Ether EPA 8260 ND gg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> Ethyl l-Butyl Ether EPA 8260 ND µg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> Methyl-t-Butyl Ether EPA 8260 ND µg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> t-Amyl Methyl Ether EPA 8260 ND µg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> tert-Butyl Alcohol EPA 8260 ND µg/L 50 1 50 05/20/2002 05/20/2002 <br /> Surrogate <br /> ------------------------------------- - - -------------.-.-----•--------------------_------------------------------------..-..------------------------------ <br /> Fluorobenzene EPA 8020 89.7 %Rec 1 N/A 05/20/2002 05/20/2002 <br /> { Toluene-ds EPA 8260 101.8 %Rec - 1 N/A 05/20/2002 05/20/2002 <br /> I <br /> mg/L: Milligrams/Liter(ppm) PQL: Practical Quantitation Limit H: Analyzed outside of hold time <br /> mg/Kg: Milligrams/Kilogram(ppm) DLR: Detection Limit for Reporting P: Preliminary result <br /> Ag/L: Micrograms/Liter(ppb) : PQL x Dilution S: Suspect result. See Cover Letter for comments. <br /> lag/Kg: Micrograms/Kilogram(ppb) ND:None Detected at DLR E: Analysis performed by External laboratory. - <br /> %Rec: Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: 111111[11111111111111111111111EIII1111111111111111111i1l111111111111111111uAflllli Page 5 of 7 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />