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BSKANALYTICAL <br /> LABORATORIES <br /> Tony Martin Certificate of Analysis <br /> ! Kleinfelder Inc ELAP Certificate#1180 <br /> 2825 East Myrtle Street Report Issue Date: 05/24/2002 <br /> Stockton, CA 95205-4794 <br /> BSK Submission #: 2002050830 <br /> BSK Sample ID#: 207759 <br /> I Project ID: Disco Project Desc: 2nd Qtr.G.W.Mon. <br /> Submission Comments: <br /> Sample Type: Liquid Date Sampled: 05/13/2002 <br /> iSample Description: MW-11S Time Sampled: 1420 <br /> Sample Comments: Date Received: 05/15/2002 <br /> Organics Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPN as Gasoline EPA 8015(M) 76 gg/L 50 1 50 05/20/2002 05/20/2002 <br /> i <br /> Benzene EPA 8020 0.42 pg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> i Ethylbenzene EPA 8020 ND µg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> Toluene EPA 8020 ND µg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> Total Xylenes EPA 8020 ND }tg/L 0.3 1 0.3 05/20/2002 05/20/2002 <br /> 1,2-Dibromoethane EPA 8260 ND Ag/L 5.0 1 5 05/20/2002 05/20/2002 <br /> 1,2-Dichloroethane EPA 8260 180 }Ag/L 5.0 10 50 05/21/2002 05/21/2002 <br /> Di-isopropyl Ether EPA 8260 ND Ag/L 5.0 1 5 05/20/2002 05/20/2002 <br /> Ethyl t-Butyl Ether EPA 8260 ND Ag/L 5.0 1 5 05/20/2002 05/20/2002 <br /> Methyl-t-Butyl Ether EPA 8260 ND µg/L 5.0 1 5 05/20/2002 05/20/2002 <br /> t-Amyl Methyl Ether EPA 8260 ND Ag/L 5.0 1 5 05/20/2002 05/20/2002 <br /> tent-Butyl Alcohol EPA 8260 ND Ag/L 50 1 50 05/20/2002 05/20/2002 <br /> Surrogate <br /> ---------- ------ - --- --- ---- -------------- <br /> Toluene-d8 EPA 8260 107.1 %Rec - 1 NIA 0-5/2'0/2,002-05/20/2002 <br /> LUFT Comments <br /> TPH as Gasoline fndMdual peaks inconsistent with fuel fingerprinr <br /> t <br /> mg/L:Milligrams/Liter(ppm) PQL: Practical Quantitation Limit H:Analyzed outside of hold time <br /> mg/Kg: Milligrams/Kilogram(ppm) DLR: Detection Limit for Reporting P: Preliminary result <br /> µg/L: Micrograms/Liter(ppb) : PQL x Dilution S:Suspect result. See Cover Letter for comments. <br /> f pg/Kg: Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. <br /> %Rec: Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: IIIIIkIIIIIEIIIIIIIIIIIIIIINIEIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII Page 6 of 7 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935 <br />