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BSKANALYTICAL <br /> LABORAT-ORIESI A#AENDED REPORT <br /> Tony Martin Certificate of Analysis <br /> Kleinfelder Inc ELAP Certificate#1180 <br /> 2825 East Myrtle Street Report Issue Date: 04/19/2002 <br /> Stockton, CA 95205-4794 <br /> BSK Submission#: 2002021116 <br /> BSK Sample 1D #: 185091. <br /> Project ID: DISCO Project Desc: Ist QTR 2002 GW <br /> Submission Comments: <br /> Sample Type: Liquid Date Sampled: 02/21/2002 <br /> Sample Description: SVE-North Time Sampled: 1510 <br /> Sample Comments: Date Received: 02/24/2002 <br /> Organics <br /> Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPN as Gasoline EPA 8015(M) 830 pg/L 50 1 50 03/05/2002 03/05/2002 <br /> Benzene EPA 8020 69 pg/L 0.3 1 0.3 03/05/2002 03/05/2002 <br /> Ethylbenzene EPA 8020 22 pg/L 0.3 1 0.3 03/05/2002 03/05/2002 <br /> Toluene EPA 8020 58 pg/L 0.3 1 0.3 03/05/2002 03/05/2002 <br /> Total Xylenes EPA 8020 110 pg/L 0.3 1 0.3 03/05/2002 03/05/2002 <br /> 1,2-Dibromoethane EPA 8260 ND pg/L 5.0 1 5 03/05/2002 03/05/2002 <br /> 1,2-Dichloroethane EPA 8260 20 pg/L 5.0 1 5.0 03/05/2002 03/05/2002 <br /> Di-isopropyl Ether EPA 8260 ND. pg/L 5.0 1 5 03/05/2002 03/05/2002 <br /> Ethyl t-Butyl Ether EPA 8260 ND pg/l- 5.0 1 5 03/05/2002 03/05/2002 <br /> Methyl-t-Butyl Ether EPA 8260 ND pg/L 5.0 1 5 03/05/2002 03/05/2002 <br /> t-Amyl Methyl Ether EPA 8260 ND gg/L 5.0 1 5 03/05/2002 03/05/2002 <br /> Cert-Butyl Alcohol EPA 8260 ND pg/L 50 1 50 03/05/2002 03/05/2002 <br /> Surrogate <br /> Fluonobcnzene EPA 8020 86,8 %Rec I N/A 03/05/2002 03/05/2002 <br /> Toluene-d8 EPA 8260 101.7 %Rec - I N/A 03/05/2002 03/05/2002 <br /> mg/L:Milligrams/Liter(ppm) PQL:Practical Quantitation Limit H:Analyzed outside of hold time <br /> mg/Kg:Milligrams/Kilogram(ppm) DLR:Detection Limit for Reporting P:Preliminary result <br /> pg/L:Micrograms/Liter(ppb) :PQL x Dilution S:Suspect result. See Cover Letter for comments. <br /> pg/Kg:Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. <br /> %Rec:Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: IIIIIIIINIII IIIIIIGIIIIIIIIIIIIIIIillll1111111111111HIM 111111111111011111111 Page 5 of 8 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />