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i <br /> BSKANALYTICAL <br /> LABORATORIES AMENDED REPORT <br /> 1 <br /> Tony Martin Certificate of Analysis <br /> Kleinfelder Inc ELAP Certificate#1180 <br /> 2825 East Myrtle Street Report Issue Date: 04/19/2002 <br /> Stockton, CA 95205-4794 <br /> BSK Submission#: 2002021116 <br /> BSK Sample ID#: 185090 <br /> Project ID. DISCO Project Desc: 1st QTR 2002 GW <br /> Submission Comments: <br /> Sample Type: Liquid Date Sampled: 02/21/2002 <br /> Sample Description: SVE-South Time Sampled: 1437 <br /> Sample Comments: Date Received: 02/24/2002 <br /> Organics PCep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) 120000 µg/L 50 200 10000 03/06/2002 03/06/2002 <br /> ` Benzene EPA 8020 6300 µg/L 0.3 200 60 03/06/2002 03/06/2002 <br /> Elhylbenzene EPA 8020 3500 µg/L 0.3 200 60 03/06/2002 0.3/06/2002 <br /> Toluene EPA 8020 18000 gg/L 0.3 400 120 03/07/2002 03/07/2002 <br /> Total Xylenes EPA 8020 22000 µg/L 0.3 200 60 03/06/2002 03/06/2002 <br /> 1,2-Dibromoelhane EPA 8260 480 Ag/L 5.0 10 50 03/05/2002 03/05/2002 <br /> 1,2-Dichloroethane EPA 8260 960 µg/L 5.0 50 250 03/06/2002 03/06/2002 <br /> Di-isopmpyl Ether EPA 8260 ND µg/L 5.0 10 50 03/05/2002 03/05/2002 <br /> Ethyl t-Butyl Ether EPA 8260 ND µg/L 5.0 10 50 03/05/2002 03/05/2002 <br /> Methyl-t-Butyl Ether EPA 8260 ND gg/L 5.0 10 50 .03/0512002 03/05/2002 <br /> t-Amyl Methyl Ether EPA 8260 ND µg/L 5.0 10 50 03/05/2002 03/05/2002 <br /> tert-Butyl Alcohol EPA 8260 ND µg/L 50 10 500 03/05/2002 03/05/2002 <br /> Surrogate <br /> Fluorobenzene EPA 8020 88,8 %Rec - 200 N/A 03/06/2002 03/06/2002 <br /> Toluene-d8 EPA 8260 95.2 %Rec - 10 N/A 03/05/2002 03/05/2002 <br /> mg/L:Milligrams/Liter(ppm) PQL:Practical Quantitation Limit H:Analyzed outside of hold time <br /> mg/Kg: Milligrams/Kilogram(ppm) DLR:Detection Limit for Reporting P:Preliminary result <br /> µg/L:Micrograms/Liter(ppb) :PQL x Dilution S.Suspect result. See Cover Letter for comments. <br /> Ag/Kg:Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. <br /> %Roc:Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: III0IIIIIIII1111II1111IIIIIIIII1111111111I111IIIIIIIIII111IIIIIIIIII1IN11IIIIIIIIiIIIHII Page 4 of 8 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,1n CA 800-877-8310 Fax 559-485-6935 <br />