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BSKANALYTICAL <br /> LABOR.ATOIRIES <br /> I <br /> Tony Martin Certificate of Analysis <br /> Kleinfelder Inc ELAP Certificate #1180 <br /> 2825 East Myrtle Street <br /> Report Issue Date: 0 31 1 512002 <br /> Stockton, CA 95205-4794 <br /> I <br /> BSK Submission #: 2002021116 <br /> BSK Sample ID #: 185092 <br /> Project ID: DISCO Project Desc: 1st QTR 2002 GW <br /> Submission Comments: <br /> Sample Type: Liquid Date Sampled: 02/21/2002 <br /> Sample Description: NPI-70` Time Sampled: 1542 <br /> Sample Comments: Date Received: 02/24/2002 <br /> Organics <br /> Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) 100000 gg/L 50 40 2000 03/06/2002 03/06/2002 <br /> Benzene EPA 8020 5600 µglL 0.3 400 120 03/07/2002 03/07/2002 <br /> Etlhylbenzene EPA 8020 4000 µg/L 0.3 400 120 03/07/2002 03/07/2002 <br /> Toluene EPA 8020 26000 µg/L 0.3 400 120 03/07/2002 03/07/2002 <br /> Total xylenes EPA 8020 25000 µg/L 0.3 400 120 03/07/2002 03/07/2002 <br /> 1,2-Dibromoethane EPA 8260 60 ug/L 5.0 5 25 03/05/2002 03/06/2002 <br /> 1,2-Dichlomethane EPA 8260 1000 µg/L 5.0 5 25 03/05/2002 03/06/2002 <br /> tert-Butyl Alcohol EPA 8260 ND µg/l, 50 5 250 03/05/2002 03/06/2002 <br /> Surrogate <br /> -•----------------------------------------- --------------------------- <br /> Fluorobenzene EPA eoz0 82,6 %Rec - 400 N/A 03/07/2002 03/07/2002 <br /> {I Toluene-0 EPA 8260 73,2 %Ree - 5 - N/A 03/05/2002 03/06/2002 <br /> I . <br /> mg/L:Milligrams/Liter(ppm) PQL:Practical Quantitation Limit H:Analyzed outside of hold time <br /> mg/Kg:Milligrams/Kilogram(ppm) DLR: Detection Limit for Reporting P:Preliminary result <br /> }tg/L:Micrograms/Liter(ppb) : PQL x Dilution S:Suspect result. See Cover Letter for comments. <br /> pg/Kg:Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. <br /> %Rec: Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: 1111111111111111iIIIlI111111111161111111111111111111111111111111111111111111111111111 loll 11111111 6 of 8 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />