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J <br /> BSKANALYTICAL <br /> LABORATORIES <br /> Tony Martin Certificate of Analysis <br /> Kleinfelder Inc ELAP Certificate#1180 <br /> 2825 East Myrtle Street Report Issue Date: 03/14/2002 <br /> Stockton, CA 95205-4794 <br /> BSK Submission#: 2002021116 <br /> BSK Sample ID#: 185093 <br /> Project ID: DISCO Project Desc: 1st QTR 2002 GW <br /> Submission Comments: <br /> Sample Type: Liquid Date Sampled: 02/21/2002 <br /> Sample Description: NPI-80' Time Sampled:. 1600 <br /> Sample Comments: Date Received: 02/24/2002 <br /> Organics Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) 180000 Rg/L 50 40 2000 03/06/2002 03/06/2002 <br /> Benzene EPA 8020 26000 Ag/L 0.3 400 120 03/07/2002 03/07/2002 <br /> Ethylbenzene EPA 8020 3900 Ag/L 0.3 400 120 03/07/2002 03/07/2002 <br /> Toluene EPA 8020 50000 Ag/L 0.3 400 120 03/07/2002 03/07/2002 <br /> Total Xylenes EPA 8020 21000 Rg/L 0.3 400 120 03/07/2002 03/07/2002 <br /> 1,2-Dibromoethane EPA 8260 1000 lug/l. 5.0 50 250 03/06/2002 03/07/2002 <br /> 1,2-Dichloroethane EPA 8260 1900 µg/L 5.0 SO 250 03/06/2002 03/07/2002 <br /> tert-Butyl Alcohol EPA 8260 ND Ag/l- 50 10 500 03/05/2002 03/06/2002 <br /> Surrogate <br /> ----------------------------------------------------•------------------------------------------------------------------------................... ----..----------------------- <br /> Fluorobenzene EPA 8020 81.2 °/u Rec - 400 N/A 03/07/2002 03/07/2002 <br /> Toluene-d8 EPA 8260 75.4 %Rec 10 N/A 03/05/2002 03/06/2002 <br /> 1 . <br /> mg/L:Milligrams/Liter(ppm) PQL:Practical Quantitation Limit H:Analyzed outside of hold time <br /> mg/Kg:Milligrams/Kilogram(ppm) DLR:Detection Limit for Reporting P:Preliminary result <br /> i Ag/L:Micrograms/Liter(ppb) :PQL x Dilution S:Suspect result. See Cover Letter for comments. <br /> gg/Kg:Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. <br /> %Rec:Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: I lllfllllllllllillllllllll 1111111lIIIIIlIIIIIIIIIIIIIIIIIIIII III!lIIIIIIIIIIIIlllllllllllllllll Page 7 of 8 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />