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r i t t t t t t t r r t r t t t r r t <br /> Torrent Laboratory, Inc. nate: 09-Apr-04 <br /> CLIENT: PG&E Technical and Ecological Services(T ANALYTICAL QC SUMMARY REPORT <br /> Work Order: 0404009 <br /> Project: TestCode: 8260S <br /> Sample ID BLANK-1 D SampType: MBLK TestCode: 8260_S Units: jig/Kg Prep Date: 417/2004 Run ID: VOCGCMSI-040407A <br /> Client ID: 7.7_777 Batch ID: R3206 TestNo: SW8260B Analysis Date: 4/712004 SegNo: 46398 <br /> Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> Benzene ND 10 <br /> Ethyl tert-butyl ether(ETBE) ND 10 <br /> Ethylbenzene ND 10 r <br /> Isopropyl ether(IPE) ND 10 <br /> Methyl tert-butyl ether(MTBE) ND 10 <br /> t-Butyl alcohol(t-Butanol) ND 50 <br /> tert-Amyl methyl ether(TAME) ND 10 <br /> Tetrachloroethene ND 10 <br /> Toluene ND 10 <br /> Xylenes,Total ND 10 <br /> Surr:4-Bromofluorobenzene 35.81 0 50 0 71.6 65 135 0 0 <br /> Surr: Dibromofluoromethane 41.26 0 50 0 82.5 65 135 0 0 <br /> Surr:Toluene-d8 41.68 0 50 0 83.4 65 135 0 0 <br /> Sample ID LCS-1,50 PPB SampType: LCS TestCode: 8260_S Units: pg/Kg Prep Date: 41712004 Run ID: VOCGCMSI_040407A <br /> Client ID: 7.7.777 Batch ID: R3206 TestNo: SW8260B Analysis Date: 4/7/2004 SegNo: 46399 <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowL[mit HighLimit RPD Ref Val %RPD RPDLimit Qua[ <br /> Benzene 43.67 10 50 0 87,3 70 130 0 0 <br /> Toluene 49.67 10 50 0 99.3 70 130 0 0 <br /> Surr:4-Bromofluorobenzene 41.53 0 50 0 83.1 65 135 0 0 <br /> Surr:Dibromofluoromethane 47 0 50 0 94 65 135 0 0 <br /> Surr:Toluene-d8 49.99 0 50 0 100 65 135 0 0 <br /> Sample ID LCSD-1,50 PPB SampType: LCSD TestCode: 8260_S Units: pg/Kg Prep Date: 417!2004 Run ID: VOCGCMSI 040407A <br /> Client ID: 7777 Batch ID: R3206 TestNo: SW8260B Analysis Date: 417!2004 SegNo: 46400 <br /> Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] <br /> Benzene 45.22 10 50 0 90.4 70 130 43.67 349 30 <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank <br /> J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits Page 1 of 4 <br />