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CLIENT: PG&E Technical and Ecological Services(T ANALYTICAL QC SUMMARY REPORT Work Order: 0404009 Project: TestCode: 8260S Sample ID LCSD-1,50 PPB SampType: LCSD TestCode: 8260_S Units: pg/Kg Prep Date: 4/712004 Run ID: VOCGCMSi_040407A Client ID: 7777 Batch ID: R3206 TestNo: SW8260B Analysis Date: 417/2004 SegNo: 46400 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Toluene 52.75 10 50 0 106 70 130 49.67 6.01 30 Surr:4-Bromofluorobenzene 44.73 0 50 0 89.5 65 135 0 0 0 Surr:Dibromofluoromethane 50.92 0 50 0 102 65 135 0 0 0 Surr.Toluene-d8 54.2 0 50 0 108 65 135 0 0 0 r Sample ID 0404009-003AMS SampType: MS TestCode: 8260_S Units: pg/Kg Prep Date: 4/712004 Run ID: VOCGCMSI_040407A ` Client ID: DPI-9 Batch ID: 83206 TestNo: SW0260B Analysis Date: 4/7/2004 SegNo: 46393 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Benzene 43.31 10 50 0 86.6 70 130 0 0 Toluene 51.79 10 50 0 104 70 130 0 0 Surr:4-Bromofluorobenzene 45.87 0 50 0 91.7 65 135 0 0 Surr:Dibromofluoromethane 51.79 0 50 0 104 65 135 0 0 Surr.Toluene-d8 52.51 0 50 0 105 65 135 0 0 Sample ID 0404009-003AMSD SampType: MSD TestCode: 8260_S Units: pg/Kg Prep Date: 4f712004 Run ID: VOCGCMSI_040407A Client ID: DPI-9 Batch ID: R3206 TestNo: SW0260B Analysis Date: 41712004 SegNo: 46394 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Benzene 44.95 10 50 0 89.9 70 130 . 43.31 3.72 30 Toluene 54.64 10 50 0 109 70 130 51.79 5.36 30 Surr:4-Bromofluorobenzene 44.45 0 50 0 88.9 65 135 0 0 0 Surr.Dibromofluoromethane 49.75 0 50 0 99.5 65 135 0 0 0 Surr:Toluene-d8 51.79 0 50 0 104 65 135 0 0 0 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits Page 2 of 4