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• CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Seances 2333 Shuttle Drive,Atwater CA 95301 Phone (209)384-2930 <br /> Certificate#2480 Fax (209)384-1507 <br /> BSK Analytical Laboratories Client Project ID 2003030987 Sampled 03-17-03 <br /> 1414 Stanislaus St Client Project Name Connell Motor Truck Received 03-28-03 <br /> Fresno CA 93706 Reference Number 5605 Extracted 03-28-03 <br /> Attn Miyuki Fu;ita Sample Description Soil Analyzed 03-28-03 <br /> Sample Prep/Analysis Method EPA 5030/8260 Reported 04-01-03 <br /> Lab Numbers 5605-4S, 5S 6S <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GUMS <br /> ANALYTE REPORTING SAMPLE ID SAMPLE ID SAMPLE ID <br /> LIMIT CPT2-114'SOIL CPT2-130'SOIL CPT2-92'SOIL <br /> 302908 302909 302910 <br /> (mg/Kg) (mg/K (mg/K (m/Kg) <br /> FUEL OXYGENATES <br /> Methyl tert-Butyl Ether(MTBE) 0 010 NO ND ND <br /> Di-isopropyl Ether (D1PE) 0 010 ND NO ND <br /> Ethyl tert-Butyl Ether (ETRE) 0 010 ND ND ND <br /> tert-Amyl Methyl Ether(TAME) 0 010 ND ND ND <br /> tert-Butanol(TBA) 0 800 NO ND ND <br /> VOLATILE HALOCARBON$ <br /> 1 2-Dichloroethane (1,2-DCA) 0 010 NO ND ND <br /> Ethylene Dibromide (EDB) 0 010 ND NO ND <br /> Report Limit Multiplication Factor 1 1 1 <br /> Surrogate Recoveries <br /> 1,2-Dichloroethane-d4 883% 950% 841% <br /> Toluene-d8 800% 817% 741% <br /> Instrument ID HP 5972MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit= Reporting Limit x Report Limit Multiplication Factor <br /> mg/Kg = milligrams per kilogram art per million(ppm) <br /> Ci ANALYST APPROVED BY <br /> Clary J Cone J es hillips <br /> /�Iboratory Director <br />