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• CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive Atwater,CA 95301 Phone (209)384-2930 <br /> Certificate No 2480 Fax (209)384-1507 <br /> BSK Analytical Laboratories Client Project ID 2003030987 Sampled 03-17-03 <br /> 1414 Stanislaus Street Client Project Name Connell Motor Truck Received 03-28-03 <br /> Fresno CA 93706 Reference Number 5605 Extracted 03-28-03 <br /> Attn Miyuki Finita Sample Description Water Analyzed 03-28-03 <br /> Sample Prep/Analysis Method EPA 5030/8260 Reported 04-01-03 <br /> Lab Numbers 5605-1W,2W, 3W <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GCIMS <br /> ANALYTE REPORTING SAMPLE ID SAMPLE ID SAMPLE 1D <br /> LIMIT CPT2-108' H2O CPT2-135' H2O CPT2-90' H2O <br /> 302905 302906 302907 <br /> (pg/L) /L) /L /L <br /> FUEL OXYGENATES <br /> Methyl tert-Butyl Ether(MTBE) 050 ND ND ND <br /> Di-isopropyl Ether (DIPS) 0 50 ND ND ND <br /> Ethyl tert-Butyl Ether (ETBE) 050 ND ND ND <br /> tert-Amyt Methyl Ether(TAME) 050 ND ND ND <br /> tert-Butanol(TBA) 20 ND 71 ND <br /> VOLATILE HALOCARBONS <br /> 1 2-Dichloroethane (1,2-DCA) 050 110 250 240 <br /> Ethylene Dibromide (EDB) 0 50 ND 11 ND <br /> Report Limit Multiplication Factor 2- 2- 1 <br /> Report Limit Multiplication Factor for 1,2 DCA 5 100 10 <br /> Surrogate Recoveries <br /> 1 2-Dichloroethane-d4 111% 954% 862% <br /> Toluene-d8 962% 874% 881% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit= Reporting Limit x Report Limit Multiplication Factor <br /> (pg/L) = micrograms per liter or per billion(ppb) <br /> ANALYST APPROVED BY <br /> Clan J Cone Ja C Phillips <br /> boratory Director <br />