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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone (209)384-2930 <br /> Certificate No 2480 Fax (209)384-1507 <br /> BSK Analytical Laboratories Client Project ID 2003031257 Sampled See Below <br /> 1414 Stanislaus Street Client Project Name Connell Motor Truck Received 03-28-03 <br /> Fresno CA 93706 Reference Number 5604 Extracted 03-31-03 <br /> Attn Mryuki Fu}ita Sample Description Water Analyzed 03-31-03 <br /> Sample Prep/Analysis Method EPA 503018260 Reported 0401-03 <br /> Lab Numbers 5604-1W 2W,3W,4W 5W <br /> r�kqyA!WXE <br /> GASOLINE ADDITIVES B8260 GUMS <br /> ANALYTE REPORTING SAMPLE IDSAMPLE ID SAMPLE ID SAMPLE ID <br /> LIMIT CPT3 @ 138' CPT4 @ 93' CPT4 @ 120' CPT4 @ 136' <br /> 304045304047 304048 304049 <br /> !L IL 1L !L !L <br /> FUEL 9AYGENATES <br /> Methyl tent-Butyl tither(MTBE) 050 NO NO ND ND NO <br /> Di-isopropyl Ether (DIPE) 050 NO NO NO NO ND <br /> Ethyl tert-Butyl Ether (ETRE) 050 NO NO NO ND NO <br /> tert-Amyl Methyl Ether(TAME) 050 NO NO ND NO NO <br /> Cert-Butanol(TBA) 20 NO 53 ND 42 NO <br /> VOLATILE HALOCARBONS <br /> 1 2-Dichloroethane (1 2-DCA) 050 18 95 160 220 NO <br /> Ethylene Dibromide (EDB) 050 NO NO ND ND NO <br /> Report Limit Multiplication Factor 1 1 1 1 1 <br /> Report Limit Multiplication Factor for 1,2 DCA 10 10 20 <br /> Date Sampled 03-18-03 03-19-03 03-19-03 03-19-03 03-19-03 <br /> Surrogate Recoveries <br /> 1 2-Dichloroethane-d4 958% 118% 122% 106% 111% <br /> Toluene-d8 886% 930% 934% 81 8% 790% <br /> Instrument ID MP 5972 MS <br /> Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit= Reporting Limit x Report Limit Multiplication Factor <br /> (pglL)= micrograms per liter or parts per billion(ppb) <br /> ANALYST APPROVED BY <br /> Clary J Cone Jam hrllrps <br /> L oratory Director <br />