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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone (209)384-2930 <br /> Certificate#2480 Fax (209)384-1507 <br /> BSK Analytical Laboratories Client Project ID 2003031257 Sampled See Below <br /> 1414 Stanislaus St Client Project Name Connell Motor Truck Received 03-28-03 <br /> Fresno,CA 93706 Reference Number 5604 Extracted 03-28-03 <br /> Attn Miyuki Futita Sample Description Sod Analyzed 03-28-03 <br /> Sample Prep/Analysis Method EPA 5030/8260 Reported 04-01-03 <br /> Lab Numbers 5604-9S, 10S, 11S, 12S <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GUMS <br /> ANALYTE REPORTING PL D SAMPLE ID SAMPLE 1D SAMPI ID <br /> LIMIT CPT3 @ 108 CPT3 @ 132 CPT4 @ 132 CPT4 @ 110 <br /> 304054 304055 304056 304057 <br /> m IK (mg/K (mg/K (mg/K (mg/Kg) <br /> FUEL OXYGENATES <br /> -.L <br /> Methyl tert-Butyl Ether(MTBE) 0 010 0 027 -�0 029 0 024 0 022 <br /> Di-isopropyl Ether (DIPS) 0 010 NO NO ND ND <br /> Ethyl tert-Butyl Ether (ETRE) 0 010 NO NO ND ND <br /> tert-Amyl Methyl Ether(TAME) 0 010 NO ND NO ND <br /> tert-Butanol(TSA) 0 800 NO ND NO ND <br /> VOLATILE HALOCARBONS <br /> 1,2-Dichloroethane (1 2-DCA) 0 010 NO ND ND ND <br /> Ethylene Dibromide (EDB) 0 010 NO NO ND NO <br /> Report Limit Multiplication Factor 1 1 1 1 <br /> Date Sampled 03-18-03 03-18-03 03-19-03 03-19-03 <br /> Surrogate Recoveries <br /> 1 2-Dichloroethane-d4 739% 81 8% 871% 726% <br /> Toluene-d8 736% 738% 798% 682% <br /> Instrument lD MP 5972MS <br /> Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> mg/Kg = milligrams per kilogram or parts per million(ppm) <br /> 7 <br /> iANALYST (1APPROVED BY <br /> Clary J Cone m Phdlrps <br /> Laboratory Director <br />