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Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H3021709 Date: 02/27/2003 Page: 9 <br /> Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> ' Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-8 Lab Samp ID: 33384-002 <br /> DescdLocation: MW-8 Recd Date: 02/19/2003 <br /> Sample Date: 02/14/2003 Prep Date: 02/2012003 <br /> ' Sample Time: 0953 Analysis Date: 02/20/2003 <br /> Matrix: Water QC Batch: WMS11943 <br /> Basis: Not Filtered Notes: <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.3 1. PQL 29L UGIL 1 <br /> Ethyl tert-butyl ether(ETBE) 0.5 5. PQL ND UGIL 1 <br /> tert-Amy] methyl ether(TAME) 0.3 5, PQL ND UGIL 1 <br /> Di-isopropyl ether(DIPS) 0.5 5. PQL ND UGIL 1 <br /> ' tert-Butyl alcohol (TBA) 4.6 10, PQL ND UGIL 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UGIL 1 <br /> 1,2-Dibromoethane 1 0.5 5. PQL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> ' 4-Bromofluorobenzene 65-135 SMSA 114% 1 <br /> Toluene-d8 77-150 SMEA 120% 1 <br /> 0DibromofEuoromethane 57-156 SMEAAZ 17.2% ! 1 <br /> — AZ: Sun-. recovery outside of acceptance limits due to matrix interf. <br /> i <br /> 1 <br /> 1 <br /> Approved by: IV _. ._ Date: L o <br />