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' Entech Analytical Labs Inc., la <br /> yt c, Santa Clara, CA <br /> Lab Report No.: H3021709 Date: 02/27/2003 Page: 10 <br /> Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> ' Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-9 Lab Samp ID: 33384-001 <br /> Descr/Location: MW-9 Recd Date: 02/19/2003 <br /> Sample Date: 02/14/2003 Prep Date: 02/21/2003 <br /> ' Sample Time: 0910 Analysis Date: 02121/2003 <br /> Matrix: Water QC Batch: WMS11945 <br /> Basis: Not Filtered Notes: <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 0.3 1. PQL 2Q UGIL 1 <br /> Ethyl tert-butyl ether(ETBE) 0.5 5. PQL ND UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0.3 S. PQL ND UGIL 1 <br /> Di-isopropyl ether(DIPE) 0.5 5. PQL ND UGIL 1 <br /> ' tert-Butyl alcohol (TBA) 4.6 10. PQL ND UGIL 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UG/L 1 <br /> 1,2-Dibromoethane 1 0.5 5. PQL ND UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65.135 SMEA 112% 1 <br /> Toluene-d8 77-150 SMSA 120% 1 <br /> Dibromofluoromethane 57-156 SMEAAZ 10.7% ! 1 <br /> AZ: Surr. recovery outside of acceptance limits due to matrix interf. <br /> 1 <br /> 1 <br /> Approved by: Date: �7 <br />