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Entech Analytical Labs, Inc., Santa Clara, CA <br /> ' Lab Report No.: H302i 709 Date: 02/27/2003 page: 2 <br /> ' Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-101 Lab Samp ID: 33384-009 <br /> Descr/Location: MW-101 Rec'd Date: 02/19/2003 <br /> Sample Date: 02/14/2003 Prep Date: 02/2012003 <br /> ' Sample Time. 1526 Analysis Date: 02/20/2003 <br /> Matrix: Water QC Batch: WMS11943 <br /> Basis: Not Filtered Notes: <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-ter#-butyl ether(MTBE) 0.3 1. PQL NO UGIL 1 <br /> ' Ethyl tert-butyl ether(ETBE) 0.5 5. PQL NO UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL NO UGIL 1 <br /> Di-isopropyl ether(DIPS) 0.5 5. PQL ND UGIL 1 <br /> ' tert-Butyl alcohol (TBA) 4.6 10. PQL NO UGIL 1 <br /> 1,2-Dichloroethane 0.3 5. PQL NO UGIL 1 <br /> 1,2-Dibromoethane 0.5 5. PQL_[_ NO UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluarobenzene 65-135 SMEA 111% 1 <br /> Toluene-d8 77-150 SMEA 122% 1 <br /> Dibromofluoromethane 57-156 SMEAAZ 0% ! 1 <br /> AZ: Surr. recovery outside of acceptance limits due to matrix interf. <br /> Approved by: �- .. Date: <br /> L9�7 <br /> .f <br />