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Quality Control Results <br /> ' Client: Earth Tech, Inc. Job Number: 720-14844-1 <br /> Lab Control Spike/ Method: 8270C <br /> Lab Control Spike Duplicate Recovery Report-Batch: 720-37157 Preparation: 3550B <br /> ' LCS Lab Sample ID: LCS 720-37157/2-A Analysis Batch: 720-37270 Instrument ID: Sat 2K1 <br /> Client Matrix: Solid Prep Batch: 720-37157 Lab File ID: d:\data\200806\062408\lcs <br /> Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 30.01 g <br /> ' Date Analyzed: 06/24/2008 1725 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/23/2008 1506 Injection Volume: 1.0 uL <br /> LCSD Lab Sample ID:LCSD 720-37157/3-A Analysis Batch: 720-37270 Instrument ID: Sat 2K1 <br /> Client Matrix: Solid Prep Batch: 720-37157 Lab File ID: d:\data\200806\062408\lcsd <br /> Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 30.05 g <br /> 1 Date Analyzed: 06/24/2008 1759 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/23/2008 1506 Injection Volume: 1.0 uL <br /> % Rec. <br /> Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual <br /> 2,4-Dinitrophenol _ 62 50 21 -96 23 35 <br /> ' 4-Nitrophenol 89 84 54- 125 6 35 <br /> Dibenzofuran 81 74 55-100 9 35 <br /> 2,4-Dinitrotoluene 85 89 57- 110 4 35 <br /> ' 2,6-Dinitrotoluene 87 88 54- 119 1 35 <br /> Diethyl phthalate 87 79 49- 117 10 35 <br /> 4-Chlorophenyl phenyl ether 81 83 57-103 2 35 <br /> Fluorene 81 82 54-104 1 35 <br /> ' 4-Nitroaniline 85 90 59-114 5 35 <br /> 2-Methyl-4,6-dinitrophenol 80 81 48-111 1 35 <br /> N-Nitrosodiphenylamine 75 81 56- 105 7 35 <br /> 4-Bromophenyl phenyl ether 83 81 53-101 3 35 <br /> Hexachlorobenzene 81 81 55- 105 0 35 <br /> Pentachlorophenol 65 70 35-90 7 35 <br /> Phenanthrene 74 84 54- 100 12 35 <br /> ' Anthracene 74 87 55-101 16 35 <br /> Di-n-butyl phthalate 82 86 55-102 5 35 <br /> Fluoranthene 76 82 54-102 8 35 <br /> Pyrene 67 69 48-91 3 35 <br /> Butyl benzyl phthalate 67 73 53-98 9 35 <br /> 3,3'-Dichlorobenzidine 60 59 42-87 2 35 <br /> Benzo[a]anthracene 71 74 55-91 3 35 <br /> Bis(2-ethylhexyl)phthalate 67 71 53-98 5 35 <br /> ' Chrysene 64 64 49-96 0 35 <br /> Di-n-octyl phthalate 69 71 53-91 4 35 <br /> Benzo[b]fluoranthene 76 91 56-105 18 35 <br /> Benzo[a]pyrene 72 81 55-102 12 35 <br /> Benzo[k]fluoranthene 75 77 51 -93 3 35 <br /> Indeno[1,2,3-cd]pyrene 96 102 56- 110 6 35 <br /> Benzo[g,h,i]perylene 89 96 56-106 8 35 <br /> Benzoic acid 22 12 8-35 56 35 <br /> Azobenzene 78 87 52- 100 11 35 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> ' TestAmerica San Francisco Page 21 of 30 <br />