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Ge(,. analytical Laboratories, inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209)572-0916 <br /> Report# P007-21 CERTIFICATE OF ANALYSIS Date: 1/13/03 <br /> Thorpe Oil Date Rec'd: 1/07/03 <br /> Date Started: 1/10/03 <br /> PO Box 357 Project: S.T.Service-3505 Navy Dr. Stockton,Ca. Date Completed:1/10/03 <br /> Lodi CA 95241 <br /> Date Sampled: 1/07/03 <br /> PO# Time: <br /> Sample ID: Stockpile 1-A Thru 1-C Sampler : R.Azevedo(Geo) <br /> Lab ID: P200055 Thru P200057 <br /> Method RL Analyte Results Units <br /> 8260B 10 Methyl tert-butyl ether(MTBE) 168 µg/Kg <br /> 400 Ethanol ND <br /> 200 tent-Butanol 532 <br /> 10 di-Isopropyl ether(RIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> 10 Ethylene dibromide(EDB) ND <br /> 5.0 t.hane(1,2-DCA) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 20 24.4 122.0 66-133 <br /> 2-Bromo-l-chloropropane 20 22.0 110.0 63-139 <br /> 4-Bromofluorobenzene 20 19.8 99.0 64-136 <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />