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Geoi-inalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# P007-21 Date: 1/13/03 <br /> Thorpe Oil Project: S.T.Service-3505 Na Dr. Stockton,Ca. Date Recd: 1/07/03 <br /> Navy Date Started: 1/09/03 <br /> PO Box 357 Date Completed:1/10/03 <br /> Lodi CA 95241 PO# <br /> Date Sampled: 1/07/03 <br /> Sampler: R.Azevedo(Geo) <br /> Sample ID Lab ID RL Method Analyte Results Units <br /> TK1@12' P200054 5.0 8021B Benzene ND pg/Kg <br /> 5.0 Toluene ND pg/Kg <br /> 5.0 Ethyl Benzene ND pg/Kg <br /> 5.0 Total Xylenes ND pg/Kg <br /> 10 8260B Methyl tert-Butyl Ether 90 pg/Kg <br /> 1.0 5(W Luft Gasoline ND mg/Kg <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> a,a,a-TFT 250 198 79.20 66-117 <br /> *MTBE confirmed by 8260B <br /> Stockpile 1-A Thru 1-C P200055 5.0 8021B Benzene ND pg/Kg <br /> Thru 5.0 Toluene ND pg/Kg <br /> P200057 5.0 Ethyl Benzene ND jig/Kg <br /> 5.0 Total Xylenes ND pg/Kg <br /> 10 8260B Methyl tert-Butyl Ether 168 lig/Kg <br /> 1.0 5030 Luft Gasoline ND mg/Kg <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> a,a,a-TFT 250 246 98.40 66-117 <br /> *MTBE confirmed by 8260B <br /> 4 <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification 2157 Laboraton, Director <br />