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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htlp.//www.mccm ell cam E-mail matn@mecampbel] corn <br /> Advanced GeoEnvironmental Client Project ID Larry Auto Date Sampled 08/12/99 <br /> 4005 North Wilson Way Date Received 08/13/99 <br /> Stockton,CA 95205 Client Contact Kevm McKibben Date Extracted 08/16-08/17/99 <br /> Client P O Date Analyzed 08116-08117199 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> I Lab ID 17162 <br /> Client ID MW-3 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> I Acetone 120 trans-l,3-Dichloropropene ND <br /> Benzene 24 Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene 12 <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND Iodomethane ND <br /> Bronioform ND Isopropylbenzene 12 <br /> Bromomethane ND p-Isopropyl toluene ND <br /> I n-Butyl benzene ND Methyl butyl ketone ND <br /> sec-Butyl benzene ND Methylene Chloride— ND <br /> tent-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide ND Methyl isobutyl ketone c ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) -- <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Etbe ND Styrene ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane 2 9 1,1,2,2-Tetrachloroethane ND <br /> 2-Cblorotoluene ND Termchloroethene ND<3 <br /> 4-Chlorotoluene ND Toluene"' 15 <br /> Dibromochloromethane ND 1,2,3-Tnchlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Tnchlorobenzene ND <br /> Dibromomethane ND 1,1,1-Tnchloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Tnchloroethane ND <br />' 1,3-Dichlorobenzene ND Tnehloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Tnchloropropane ND <br /> 1,1-Dichlorocthane ND 1,2,4-Tnmethylbenzene ND <br />' 1,2-Dichloroethane 2 0 1,3,5-Trimethylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate 13 <br /> cis-1,2-Dichloroethene ND Vinyl Chloride'° ND <br /> trans-l,2-Dichloroethene ND Xylenes,total 33 <br />' 1,2-Dichloropropane ND Comments <br /> 1,3-Dichloropropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluorometbane 88 <br />' 1,1-Dichloropropane ND Toluene-d8 103 <br /> cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 89 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,%%ipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-bulanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, p) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton, Lab Director <br /> 1 <br />