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110 2nd Avenue South,#ED7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> I ��C/// hbtW://www,mccarnpbell,com E-mail main@mecampbell com <br /> f <br /> Advanced GeoEnvironmental Client Project ID Larry Auto Date Sampled 08/12/99 <br /> 4005 North Wilson Way Date Received 08/13/99 <br /> IStockton, CA 95205 Client Contact Kevin McKibben Date Extracted 08116-08/17/99 <br /> Client P 4 Date Analyzed 08116-08/17/99 <br /> I Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 17163 <br /> Client 1D MW-7 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone @ ND<50 trans-1,3-Dichloropropene NIX17 <br /> Benzene 310 Ethylene dibromide ND<17 <br /> Brornobenzene ND<17 Ethylbenzene 57 <br /> Bromochloromethane ND<17 liexachlorobutadiene ND<17 <br /> Bromodichloromethane NIX17 lodornethane ND<17 <br /> Bromoform ND<17 ]sopropylbenzene ND<17 <br /> Bromomethane NDS17 p-Isopropyl toluene ND<17 <br /> n-Butyl benzene ND<17 Methyl bury]ketone ND<l 7 <br /> sec-Butyl benzene ND<17 Methylene Chloride` ND<17 <br /> tert-Butyl benzene ND<17 Methyl ethyl ketone NIX17 <br /> Carbon Disulfide ND<17 Methyl isobutyl ketone ND<17 <br /> Carbon Tetrachloride NIX17 Methyl tent-Butyl Ether(MTBE) --- <br /> Chlorobenzene NIK17 Naphthalene ND<17 <br /> Chloroethane ND<17 n-Propyl benzene NIX17 <br /> 2-Chloroethyl Vinyl Ether"' ND<17 Styrene W ND<17 <br /> Chloroform ND<17 1,1,1,2-Tetr2chloroethane ND<17 <br /> Chloromethane ND<17 1,1,2,2-Tetrachloroethane NIX17 <br />' 2-Chlorotoluene ND<17 Tetrachloroethene ND<17 <br /> 4-Chlorotoluene ND<17 Toluene"1 470 <br /> Dibromochloromethane ND<17 1,2,3-Tnchlorobenzene ND<l 7 <br /> 1,2-Dibrorno-3-chloropropane NDS17 1,2,4-Tnchlorobenzene NIXI7 <br />' Dibromomethane ND<17 1,1,1-Tnchloroethane NIX]7 <br /> 1,2-Dichlorobenzene NDS 17 1,1,2-Tnchloroethane ND<17 <br /> 1,3-Dichlorobenzene ND<17 Trichloroethene ND<17 <br />' 1,4-Dichlorobenzene ND<17 Trichlorofluoromethane ND<17 <br /> Dichlorodifluoromethane ND<17 1,2,3-Tnchloropropane ND<l7 <br /> I,1-Dichloroethane ND<17 1,2,4-Trimethylbenzene 32 <br /> 1,2-Dichloroethane ND<17 1,3,5-Tnmethylberizene ND<17 <br />' 1,1-Dichloroethene NIX17 Vinyl Acetate ° NIX17 <br /> cis-1,2-Dichloroethene ND<17 Vinyl Chloride NIX17 <br /> trans-] 2-Dichloroethene ND<17 Xylenes,total 300 <br /> 1,2-Dichloropropane ND<17 Comments <br />' 1,3-Dichloropropane ND<17 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<17 Dibromofluoromethane 104 <br /> 1,1-Dichloropropene ND<17 Toluene-d8 106 <br /> cis-1,3-Dichloropropene ND<17 4-Bromofluorobenzene 96 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Repotting limits unless otherwise stated nater samples 1 ug/L,vapor samples 0 5 ug(L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />