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' 110 2nd Avenue South,#D7,Pacheco,CA 9455 3-55 60 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htW,b5_n.mc0mprslj corn E-mail main@mccampbell com <br /> 1 <br /> Advanced GeoEnvironmental Client Project ID Larry Auto Date Sampled 08/12/99 <br />' 4005 North Wilson Way Date Received 08/13/99 <br />' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 08116-08/17/99 <br /> Client P O Date Analyzed 08116-08117/99 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 17164 <br />' Client ID VW-2B <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<230 trans-1,3-Dichloropropene ND<500 <br />' Benzene 24,000 Ethylene dibromide ND<500 <br /> Bromobenzene ND<500 Ethylbenzene 1800 <br /> Bromochloromethane ND<500 Hexachlorobutadlene ND<500 <br /> Bromodichloromethane ND<500 lodomethane ND<500 <br />' Bromoform ND<500 Isopropylbenzene ND<500 <br /> Brornomethane ND<500 p-Isopropyl toluene ND<500 <br /> n-Butyl benzene ND<500 Methyl butyl ketoneND<500 <br /> sec-Butyl benzene ND<500 Methylene Chloride` ND<570 <br />' tert-Butyl benzene ND<500 Methyl ethyl ketone ND<500 <br /> Carbon Disulfide ND<500 Methyl isobuty]ketone 19ND<500 <br /> Carbon Tetrachloride ND<500 Methyl tert-Butyl Ether(MTBE) -- <br /> Chlorobenzene ND<500 Naphthalene ND<500 <br /> Chloroethane ND<500 n-Propyl benzene ND<500 <br /> 2-Chlorcethyl Vinyl Ethe NDt500 Styrene NIK500 <br /> Chloroform ND<500 1,1,1,2-Tetrach]oroethane ND<500 <br /> Chloromethane ND<500 1,1,2,2-Tetrachloroethane ND<500 <br />' 2-Chlorotoluene ND<500 Tetrachloroethane ND<500 <br /> 4-Chlorotoluene ND<500 Toluene"1 17,000 <br /> Dibromochlorometbane ND<500 1,2,3-Tnchlorobenzene ND<500 <br />' 1,2-Di1romo-3-chloroprop2ne ND<500 1,2,4-Tnchlorobenzene ND<500 <br /> Dibromomethane ND<500 1,1,1-Trichloroethane ND<500 <br /> 1,2-Dichlorobenzene ND<500 1,1,2-Trichloroethane ND<500 <br /> 1,3-Dichlorobenzene ND<500 Tnchloroethene ND<500 <br />' 1,4-Dic11101"obenzene ND<500 Trichlorofluoromethane ND<500 <br /> Dichlorodifluoromethane ND<500 1,2,3-Tnchloropropane ND<500 <br /> l,l-Dichloroethane ND<500 1,2,4-Trimethylbenzene 1300 <br /> 1,2-Dichloroethane 1600 1,3,5-Tnmethylbenzene ND<500 <br />' <br /> 1,1-Dichloroethene ND<500 Vinyl Acetate " ND<500 <br /> cis-1,2-Dichloroethene ND<500 Vinyl Chloride"I ND<500 <br /> trans-l,2-Dichlomethene ND<500 Xylenes,total 9700 <br /> 1,2-Dichloropropane ND<500 Comments <br />' 1,3-Dichloropropane ND<500 Surrogate Recok cries(%) <br /> 2,2-Dichloropropane ND<500 Dibromofluoromethane 98 <br /> 10-Dichloropropene ND<500 Toluene-d8 102 <br /> cis-1,3-Dichloropropen e ND<500 4-Bromofluorobenzene 101 <br />' water and vapor samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples I ug/E vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/w1pe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br />' (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (b)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 _Z/7 Edward Hamihon,Lab Director <br />