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]10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> /www.mccamobell c4m E-mail main@rnccampbell coin <br />' Advanced GeoEnvironmental Client Protect ID Larry Auto Date Sampled 08/12/99 <br /> 4005 North Wilson Way Date Received 08/13/99 <br /> 1 Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 08/16-08/17/99 <br /> Client P O Date Analyzed 08/16-08/17/99 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 17166 <br />' Client ID VW-4 <br /> Matrix W <br /> Compound Concentration* Compound Concentration" <br /> Acetone f ND trans-l,3-Dichloropropene ND<500 <br />' Benzene 17,000 Ethylene dibmmide ND<500 <br /> Bromobenzene ND<500 Ethylbenzene 3100 <br /> Bromochloromethane ND<500 Hexachlorobutadicne ND<500 <br /> Bromodichloromethane ND<500 lodomethane ND<500 <br /> Bromoform ND<500 isopropylbenzene ND<500 <br /> Bromomethane ND<500 p-Isopropyl toluene NIK500 <br /> n-Butyl benzene ND<500 Methyi butyl ketone ND<500 <br /> Sec-Butyl benzene ND<500 Methylene Chloride(.) ND<500 <br />' tert-Butyl benzene ND<500 Methyl ethyl ketone ND<500 <br /> Carbon Disulfide ND<500 Methyl isobutyl ketone ND<500 <br /> Carbon Tetrachloride ND<500 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<500 Naphthalene ND<500 <br /> Chloroethane ND<500 n-Propyl benzene ND<500 <br /> 2-Chloroethyl Vinyl Ether` ND<500 Styrene ND<500 <br /> Chloroform ND<500 1,1,1,2-Tetrachloroethane ND<500 <br /> Chloromethane ND<500 1,1,2,2-Tetrachloroethane ND<500 <br /> 2-Chlorotoluene ND<500 Tetrachloroethene ND<500 <br /> 4-Chlorotoluene ND<500 Toluene W 16,000 <br /> Dibromochloromethane ND<500 1,2,3-Trichlorobenzene ND<500 <br />' 1,2-Dibromo-3-chloroprop2ne ND<500 1,2,4-Tnchlorobenzene ND<500 <br /> Dibromomethane ND<500 1,1,1-Tn chloroethane ND<500 <br /> 1,2-Dichlorobenzene ND<500 1,1,2-Trichloroethane ND<500 <br /> 1,3-Dichlorobenzene ND<500 Tnchloroethene ND<500 <br />' 1,4-Dichlorobenzene ND<500 Trichlorofluoromethane ND<500 <br /> Dichlorodifluoromethane ND<500 1,2,3-Tnchloropropane ND<500 <br /> 1,1-Dichloroethane ND<500 1,2,4-Tn mcthyibenzene 2800 <br /> 1,2-Dichloroethane 900 1,3,5-Trimethyibenzene 880 <br />' i,]-Dichloroethene ND<500 Vinyl Acetate") ND<500 <br /> cis-1,2-Dichloroethene ND<500 Vinyl Chloride ° ND<500 <br /> trans-l,2-Dichloroethene ND<500 Xylenes,total 17,000 <br /> 1,2-Dichloropropane ND<500 Comments <br /> 1,3-Dichloropropane ND<500 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<500 Dibromoffuoromethane 105 <br /> ],1-Dichloropropcne ND<500 I Toluene-d8 107 <br /> cis-],3-Dichloropropene ND<500 4-Bromoiluorobcnzene 110 <br />' 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton,Lab Director <br /> 1 <br />