]10 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> MCCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> /www.mccamobell c4m E-mail main@rnccampbell coin
<br />' Advanced GeoEnvironmental Client Protect ID Larry Auto Date Sampled 08/12/99
<br /> 4005 North Wilson Way Date Received 08/13/99
<br /> 1 Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 08/16-08/17/99
<br /> Client P O Date Analyzed 08/16-08/17/99
<br />' Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 17166
<br />' Client ID VW-4
<br /> Matrix W
<br /> Compound Concentration* Compound Concentration"
<br /> Acetone f ND trans-l,3-Dichloropropene ND<500
<br />' Benzene 17,000 Ethylene dibmmide ND<500
<br /> Bromobenzene ND<500 Ethylbenzene 3100
<br /> Bromochloromethane ND<500 Hexachlorobutadicne ND<500
<br /> Bromodichloromethane ND<500 lodomethane ND<500
<br /> Bromoform ND<500 isopropylbenzene ND<500
<br /> Bromomethane ND<500 p-Isopropyl toluene NIK500
<br /> n-Butyl benzene ND<500 Methyi butyl ketone ND<500
<br /> Sec-Butyl benzene ND<500 Methylene Chloride(.) ND<500
<br />' tert-Butyl benzene ND<500 Methyl ethyl ketone ND<500
<br /> Carbon Disulfide ND<500 Methyl isobutyl ketone ND<500
<br /> Carbon Tetrachloride ND<500 Methyl tert-Butyl Ether(MTBE) ---
<br /> Chlorobenzene ND<500 Naphthalene ND<500
<br /> Chloroethane ND<500 n-Propyl benzene ND<500
<br /> 2-Chloroethyl Vinyl Ether` ND<500 Styrene ND<500
<br /> Chloroform ND<500 1,1,1,2-Tetrachloroethane ND<500
<br /> Chloromethane ND<500 1,1,2,2-Tetrachloroethane ND<500
<br /> 2-Chlorotoluene ND<500 Tetrachloroethene ND<500
<br /> 4-Chlorotoluene ND<500 Toluene W 16,000
<br /> Dibromochloromethane ND<500 1,2,3-Trichlorobenzene ND<500
<br />' 1,2-Dibromo-3-chloroprop2ne ND<500 1,2,4-Tnchlorobenzene ND<500
<br /> Dibromomethane ND<500 1,1,1-Tn chloroethane ND<500
<br /> 1,2-Dichlorobenzene ND<500 1,1,2-Trichloroethane ND<500
<br /> 1,3-Dichlorobenzene ND<500 Tnchloroethene ND<500
<br />' 1,4-Dichlorobenzene ND<500 Trichlorofluoromethane ND<500
<br /> Dichlorodifluoromethane ND<500 1,2,3-Tnchloropropane ND<500
<br /> 1,1-Dichloroethane ND<500 1,2,4-Tn mcthyibenzene 2800
<br /> 1,2-Dichloroethane 900 1,3,5-Trimethyibenzene 880
<br />' i,]-Dichloroethene ND<500 Vinyl Acetate") ND<500
<br /> cis-1,2-Dichloroethene ND<500 Vinyl Chloride ° ND<500
<br /> trans-l,2-Dichloroethene ND<500 Xylenes,total 17,000
<br /> 1,2-Dichloropropane ND<500 Comments
<br /> 1,3-Dichloropropane ND<500 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND<500 Dibromoffuoromethane 105
<br /> ],1-Dichloropropcne ND<500 I Toluene-d8 107
<br /> cis-],3-Dichloropropene ND<500 4-Bromoiluorobcnzene 110
<br />' 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe
<br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 // Edward Hamilton,Lab Director
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