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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC 'Telephone 925-798-1620 Fax 925-798-1622 <br /> ]up.//www.mccampbell.com E-mail main@mccampbell corn <br /> Date Sampled 08/12/99 <br />' Advanced GeoEnvironmental Client Protect ID Larry Auto <br /> Date Received 08/13/99 <br /> 4005 North Wilson Way <br />' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 08/16-08/17/99 <br /> Client P O Date Analyzed 08/16-08107199 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 17167 <br />' Client ID VW-5B <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<1700 trans-1,3-Dichloropropene ND<1700 <br />' Benzene 9100 Ethylene dibromide ND<1700 <br /> Bromobenzene ND<1700 Ethylbenzene 5200 <br /> Bromochloromethane ND<1700 Hexachlorobutadiene ND<1700 <br /> Bromodichloromethane NIX1700 Iodomethane NIXI 700 <br /> Brornoform ND<1700 lsopropylbenzene ND<]700 <br /> Bromomethane ND<1700 p-Isopropyl toluene ND<1700 <br /> n-Butyl benzene ND<1700 Methyl butyl ketone ND<1700 <br /> sec-Butyl benzene ND<1700 Methylene Chlonde" ND<1700 <br />' tert-Butyl benzene ND<1700 Methyl ethyl ketone` ND<1700 <br /> Carbon Disulfide ND<1700 Methyl isobutyl acetone ND<1700 <br /> Carbon Tetrachloride ND<1700 Methyl tent-Butyl Ether(MTBE) <br /> Chlorobenzene ND<1700 Naphthalene ND<1700 <br /> Chloroethane ND<1700 n-Propyl benzene ND<1700 <br /> 2-Chloroethyl Vinyl Ether" ND<1700 Styrene ifND<1700 <br /> Chloroform ND<1700 1,1,1,2-Tetrachloroe0ane ND<1700 <br /> Chloromethane ND<1700 1,1,2,2-Tetrachl oroethan e ND<1700 <br />' 2-Chlorotoluene ND<1700 Tetrachloroethene ND<l700 <br /> 4-Chlorotoluene ND<1700 Toluene'"" 41,000 <br /> Dibromochloromethane ND<1700 1,2,3-Trichlorobenzene ND<1700 <br /> 1,2-Dibromo-3-chloropropane ND<l700 1,2,4-Tnchloroben2ene ND<l700 <br /> Dibromomethane ND<1700 1,1,t-Tnchl oroethane ND<1700 <br /> 1,2-Dichlorobenzene ND<1700 1,1,2-Tnchloroethane ND<1700 <br /> 1,3-Dichlorobenzene ND<1700 Trichloroethene ND<1700 <br /> 1,4-Dichlorobenzene ND<1700 Tnchlorofluoromethane ND<1700 <br /> Dichlorodifluoromethane N D<1700 1,2,3-Tnchl oropropane ND<1700 <br /> 1,1-Dichlomethane ND<1700 1,2,4-Trimethylbenzene 3600 <br /> 1,2-Dichloroethane ND<1700 1,3,5-Tnmethylbenzene ND<1700 <br /> ],1-Dichloroethene ND<1700 Vinyl Acetate'"' ND<1700 <br /> cis-1,2-Dichloroethene ND<1700 Vinyl Chloride ° ND<1700 <br /> trans-1,2-Dichloroethene -ND<1700 Xylenes,total 29,000 <br /> 1,2-Dtchloropropane ND<1700 Comments <br /> 1 1,3-Dichloropropane ND<1700 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<1700 Dibromofluoromethane 103 <br /> 1,3-Dichloropropene ND<1'700 Toluene-d8 106 <br /> cis-1,3-Dichloropropene ND<1700 4-BromoflUorobenzene 102 <br />' water and vapor samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, p) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton,Lab Director <br />