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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC 'Telephone 925-798-1620 Fax 925-798-1622 <br /> lain.//www,mccamphell,com E-mail tnatn@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Larry Auto Date Sampled 08/12/99 <br /> 4005 North Wilson Way Date Received 08/13/99 <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 08/16-08/17/99 <br /> Client P O Date Analyzed 08/16-08/17/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 17171 <br /> Client ID MW-1 <br />' Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<13 trans-l,3-Dichloropropene ND<13 <br />' Benzene 380 Ethylene dibromide ND<13 <br /> Bromobenzene ND<13 Ethylbenzene 80 <br /> Bromochloromethane ND<13 Hexachlorobutadiene ND<13 <br /> Bromodichloromethane ND<13 lodomethane ND<13 <br />' Bromoform ND<l 3 Isopropylbenzene ND<13 <br /> Bromomethane ND<13 p-isopropyl toluene ND<13 <br /> n-Butyl benzene ND<33 Mcthyl butyl ketone ND<13 <br /> sec-Butyl benzene ND<13 Methylene Chlonde` NFX13 <br />' tert-Butyl benzene ND<13 Methyl ethyl ketone ND<13 <br /> Carbon Disulfide ND<13 Methyl isobutyl ketone a ND<13 <br /> Carbon Tetrachloride ND<13 Methyl tert-Butyl Ether(MTBE) <br /> Chlorobenzene ND<13 Naphthalene ND<13 <br /> Chloroethane ND<13 n-Propyl benzene 19 <br /> 2-Chloroethyl Vinyl Ethe ` ND<13 Styrene ND<13 <br /> Chloroform NN 13 1,1,1,2-Tetrachloroethane ND<13 <br /> Chloromethane ND<13 1,1,2,2-Tetrachloroethane Nl <13 <br />' 2-Chlorotoluene ND<l3 Tetrachloroethene ND<13 <br /> 4-Chlorotoluene ND<13 Toluene m 130 <br /> Dibromochloromethane ND<13 1,2,3-Tnchlorobenzene ND<13 <br /> 1,2-Dibromo-3-chloropropane ND<13 1,2,4-Tnchlorobenzene ND<3 <br /> t Dibromomethane ND<13 1,1,1-Trichl oroethane ND<13 <br /> 1,2-Dichlorobenzene ND<13 1,1,2-Trichloroethane ND<13 <br /> 1,3-Dichlorobenzene ND<13 Trichloroethene ND<13 <br /> 1,4-Dichlorobenzene ND<13 Tnchlorefluorotmethane ND<13 <br />' Dichlorodi fluoromethane ND<13 1,2,3-Trichloropropane ND<13 <br /> 1,1-Dichloroethane ND<13 1,2,4-Tnmethylbenzene 110 <br /> 1,2-Dichloroethane ND<13 1,3,5-Tnmcthylbenzene ND<13 <br /> 1,1-Dichloroethene ND<13 Vinyl Acetate " 33 <br /> 1 <br /> cis-1,2-Ihchloroethene ND<13 Vinyl Chloride ° ND<13 <br /> trans-l,2-Dichloroethene ND<13 Xylenes,total 230 <br /> 1,2-Dichloropropane ND<13 Comments <br />' 1,3-Dichloroprop2ne ND<13 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<13 Dibromofluoromethane 102 <br /> 1,1-Dichloropropene ND<13 Toluene-d8 104 <br /> cis-1,3-Dichloropropene ND<13 4 Bromofluorobenzene 1 98 <br /> 1 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethaim, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton, Lab Director <br />