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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MICA-WBELL ANALYTICAL INC Telephone 925-798-I620 Fax 925-798-1622 <br /> hap://www E-mail matn@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Larry Auto Date Sampled 08/12/99 <br /> 4005 North Wilson Way Date Received 08/13/99 <br /> Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 08116-008/17/99 <br /> Client P O Date Analyzed 08116-008/17/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 17170 <br /> Client ID MW-4 <br />' Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ) ND<500 trans-1,3-Dichloropropene ND<500 <br /> Benzene 19,000 Ethylene dibromide ND<500 <br /> Bromobenzene ND<500 Ethylbenzene 1500 <br /> Bromochloromethane ND<500 liexachlorobutadiene ND<500 <br /> Bromodichloromethane ND<500 lodomethane ND<500 <br /> i Bromefonn ND<500 lsopropylbenzene ND<500 <br /> Bromomethane ND<500 p-Isopropyl toluene ND<500 <br /> n-Butyl benzene ND<500 Methyl butyl ketone ND<500 <br /> sec-Butyl benzene ND<500 Methylene Chloride"' ND<500 <br />' tert-Butyl benzene ND<500 Methyl ethyl ketone ND<500 <br /> Carbon Disulfide ND<500 Methyl isobutyl ketone'' ND<500 <br /> Carbon Tetrachloride ND<500 Methyl tert-Butyl Ether(MTBE) — <br /> Chlorobenzene ND<500 Naphthalene ND<500 <br /> Chloroethane ND<500 n-Propyl benzene ND<500 <br /> 2-Chloroethyl Vinyl Ether"' ND<500 Styrene ND<500 <br /> Chloroform ND<500 1,1,1,2-Tetrachloroethane ND<500 <br /> Chloromethane NIX500 1,1,2,2-Tetrachloroethane ND<500 <br />' 2-Chlorotoluene NIx500 Tetmebloroethene ND<500 <br /> 4-Chlorotoluene ND<500 Toluene"1 13,000 <br /> Dibromochlorometbane ND<500 1,2,3-Tnchlorobenzene ND<500 <br /> 1,2-Dibromo-3-chloropropane ND<500 1,2,4-Tri chi orobenzene ND<500 <br /> Dibromometbane ND<500 1,1,1-Tn chloroethane ND<500 <br /> 1,2-Dichlorobenzene ND<500 1,1,2-Trichloroethane ND<500 <br /> 1,3-Dichlorobenzene ND<500 Tnchioroethene ND<500 <br /> 1,4-Dichlorobenzene ND<500 Trichlorofluoromethane ND<500 <br />' Dichlorodifluoromethane NIK500 1,2,3-Tnchloropropane ND<500 <br /> 1,1-Dichloroethane ND<500 i,2,4-Tnmethylbenzene 1000 <br /> 1,2-Dichloroethane 940 1,3,5-Trimethylbeiizen e ND<500 <br />' 1,1-Dichloroethene ND<500 Vinyl Acetate ° NIK500 <br /> cis-1,2-Dichloroethene ND<500 Vinyl Chloride NDX500 <br /> trans-1,2-Dichloroethene ND<500 Xylenes,total 8800 <br /> 1,2-Dichloropropane ND<500 Comments <br /> 1,3-Dichloropropane ND<500 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<500 Dibromofluoromethane 98 <br /> 1,1-Dichloropropene ND<500 I Toluene-dS 104 <br /> cis-1,3-Dichloropropene ND<500 I 4-13TOm0fluorobenzene 97 <br /> `water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor sampies 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chlaroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-but2none, (g) 4-methyl-2- <br /> pentanone or isepropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethane,(o)dimethylbenzenes <br /> DHS Cerrificahon No 1644 /� Edward Hamilton, Lab Director <br />