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145>fcDoweO e:i•a, n <br /> Sequoia . Pclal-ima,CA CA 94949 54 <br /> (707)792-1865 <br /> Analytical FAX(707)792-0342 <br /> ww w.stelaosa labs.eorn <br /> Gettler-Ryan Inc. Protect TOSCOfPHILLIPS <br /> 1364 North Mc!Jowell Blvd.,Suite B2 Project Number. 6961 l STOCKTON,C.A. Reported: <br /> Petaluma CA,94954-1116 Pro}ea Manager: Clyde Galantine 11,130/01 17:13 <br /> Total Petroleum Hydrocarbons as Gasoline and BTEX by EPA 8015M/8020M -Quality Control <br /> Sequoia Analytical - Petaluma <br /> Rgna:ng Spike Source %REC RPD <br /> Anal�,c P.esuli Limit Units Lcvel Result %REC Limits RPD Limit Notcs <br /> Batch 1110514-EPA 5030,soils <br /> 1,CS(1110514-1352) Prepared&Analyzed: 11,121/01 <br /> Gasoline(C6-02) - 5.64 1.0 mg.kg 5.50 103 65-135 <br /> Bcnzcm 0.0840 0.0050 0.0660 127 65-135 <br /> Toluene 0.403 0.0050 0.397 102 65-135 <br /> Ethylbervene 0.0907 0.0050 0.0920 99 65-135 <br /> Xylenes(total) 0.497 0.0050 0.461 108 65-135 <br /> Methyl tent-butyl ether 0.140 0050 0 105 133 65.135 <br /> Surrogate.a.a,a-Triflaororoluene 0 597 0 600 100 65-135 <br /> Surrogate. 4-Bromoflaorobencene 0.638 0 600 110 65-135 <br /> Matrix Spike(1110514-?VISI) Source:P111441-01 Prepared&Analyzed: 11/20/01 <br /> Gasoline(C6-C12) 5.66 1.0 mgkg 5.50 ND 102 65-135 <br /> Bewrne 0.0730 0.0050 0.0660 ND 111 65-135 <br /> Toluene 0.430 0.0050 0.397 ND 108 65-135 <br /> Elhylbenzen: 0.0965 0.0050 0.0920 ND 105 65-135 <br /> Xylenes(total) 0.523 0.0050 0,461 ND 113 65-135 <br /> Methyl tort-butyl ether 0.120 0.050 0.105 ND 114 65-135 <br /> Surrogate:a.0.0-Trifluorotoluene 0.621 0.640 104 65-135 <br /> Surrogate 4-Bromofluoro6enrene 0.617 0.600 103 65-135 <br /> Matrix Spike Dup(1110514-11SD1) Source: P111441-01 Prepared&Analyzed- 11/20/01 <br /> Gasoline(C6-C12 5.31 1.0 mg-'kg 5.50 ND 95 65.135 6 20 <br /> Bcn2ene 0.0762 0.0050 0.0660 ND IIS 65.135 4 20 <br /> Toluersc 0.431 0.0050 0-397 ND 108 65.135 0.2 20 <br /> Ethylbcnzcnc 0.0982 0.0050 0.0920 ND 107 65-135 2 20 <br /> Xylenes(touU 0.529 0.0050 0.461 ND 115 65-135 1 20 <br /> Mcrhyl tort-butyl ether 0.122 0.050 0.105 ND 116 65-135 2 20 <br /> Surrogate ma,a-Trifluororoluene 0623 0.6001T 104 65-135 �^ <br /> Surrogate_4-Bromofluoroben:ene 0 575 0.600 96 65-133 <br /> Sequoia Analytical-Petaluma The results in this report apply to the samples analtzed to accordance wrth the chain of <br /> custody document. Thus analyrical report must be reproduced to its entirety. <br /> Page 5 of? <br />