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Sequoia <br /> 1455 ltcDowcl]Blvd. Stc <br /> SC(�UUIa % Pctalwna.CA CA94954 <br /> 11) (707)192-1965 <br /> Analytical FAX(707)792-0342 <br /> www.wgtaoislabs.com <br /> Gcttler-Ryan Inc. Project: TOSCO/PHILLIPS <br /> 1364 North Mc Dowell Blvd.,Suite B2 Project Rumba 6981/STOCKTON,CA. Reported: <br /> Petaluma CA,94954-1116 Project Manager. Clyde Galantine 11/30/0) 17:13 <br /> Total Metals by EPA 6000/7000 Series Methods-Quality Control <br /> Sequoia Analytical-Petaluma <br /> Reporting Spike Source °kREC RPD <br /> Analyte Result Limit Units Level Result •kREC Limits RPD Limit Kaes <br /> Batch 1110616-EPA 30508 <br /> Blank(1110616-BLKI) Prepared: 11/28/01 Analyzed: 11/29/01 <br /> Lead ND 7.5 mglkg <br /> LCS(1110616-BSI) Prepared: 11/28/01 Analyzed: 11/29/01 <br /> Lead 50.6 7.S mg/kg 50.0 101 80-120 <br /> Matrix Spike(11110.6.1.6_-MSI) Source:P111449-17 Prepared: 11128/01 Analyzed: 11/29/01 <br /> Lead 55.8 7.4 mg/kg 49.0 ND 102 75-125 <br /> Matrix§01te Dep(1110616-MSDI) Source:PI11449-17 Prepared: 111 MI Analyzed: 111/29/01 <br /> bead 53.1 6.9 mg/kg 463 ND 103 75-125 5 35 <br /> Sequoia Analytical-Petaluma 71he results in this report opply to the sanp/es analysed in accordance with the chair of <br /> chuiody document.11his analytical report must be reproduced in is entirety. <br /> Page 6 of 7 <br />